{"id":40,"date":"2021-06-24T19:51:10","date_gmt":"2021-06-24T19:51:10","guid":{"rendered":"http:\/\/nmrserv.web.its.manchester.ac.uk\/nmrservice\/?page_id=40"},"modified":"2023-09-11T10:25:01","modified_gmt":"2023-09-11T10:25:01","slug":"instrumentation","status":"publish","type":"page","link":"https:\/\/nmrservice.ch.man.ac.uk\/nmrservice\/?page_id=40","title":{"rendered":"Instrumentation"},"content":{"rendered":"\n

The NMR facility in the Department of Chemistry comprises of 11 NMR spectrometers at 300\u2013600 MHz including a 400 MHz solid state instrument and a 300 MHz instrument in the undergraduate teaching laboratory.<\/p>\n\n\n\n

Bruker AVIII HD 500 \u2013 Gold<\/em> \u2013 B500 B14<\/h3>\n\n\n\n
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This instrument is equipped with a nitrogen-cooled broadband Prodigy cryoprobe. It has a sixty position SampleXpress sample changer and runs routine samples in automation 24\/7. It packs some impressive signal : noise specifications with standard samples giving ratios of 1<\/sup>H: 1350, 13<\/sup>C: 750 and 19<\/sup>F: 1200.<\/p>\n<\/div>\n<\/div>\n\n\n\n

Bruker AVIII HD 400 \u2013 Cyan<\/em> \u2013 B400 B11<\/h3>\n\n\n\n
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This instrument is equipped with a nitrogen-cooled broadband Prodigy cryoprobe. It has a sixty position SampleXpress sample changer and runs routine samples in automation 24\/7. It is used as a walk up research instrument to support high throughput analysis for chemistry researchers. Signal : noise specifications with standard samples include 1<\/sup>H: 1050, 13<\/sup>C: 475 and 19<\/sup>F: 850.<\/p>\n<\/div>\n\n\n\n

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Bruker NEO 500 \u2013 Jade<\/em> \u2013 B500 B07<\/h3>\n<\/div><\/div>\n\n\n\n
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This instrument is equipped with a range of probes for analysis of complex chemical systems and methods development. Probes include a high field-gradient probe for measurement of diffusion of large molecules, a 3-channel H-F-X probe with triaxial field gradients, and a BBFO probe for standard characterisation experiments. <\/em><\/p>\n<\/div>\n<\/div>\n\n\n\n

Bruker AVII+ 500 \u2013 Fawn<\/em> \u2013 B500 B11<\/h3>\n\n\n\n
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This 3 channel instrument is equipped with a range of probes that allow a multiple operating modes, from routine high throughput chemical analysis, to characterisation of biomolecules (including proteins), to reaction monitoring. Probes include BBI and BBFO probes for standard chemical characterisation experiments, and QXI and TXI probes for biological samples. This instrument is equipped with -120 \u00b0C to +120 \u00b0C temperature control and a Bruker InsightMR Flow Unit for reaction monitoring. <\/p>\n<\/div>\n\n\n\n

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Bruker AVIII HD 600 \u2013 Knot<\/em> \u2013 B600<\/h3>\n\n\n\n
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Situated in the Sir Robert Robinson Laboratory<\/a>, the Bruker AVIII HD 600 features a 13<\/sup>C-optimised helium-cooled cryoprobe that enables high throughput characterisation of the most complex chemical species created in the department’s laboratories. It boasts signal to noise ratios of 3200 for 1<\/sup>H and a huge 2800 for 13<\/sup>C. <\/p>\n<\/div>\n<\/div>\n\n\n\n

Bruker AVIII 400 \u2013 Solids<\/em> \u2013 B400SS<\/h3>\n\n\n\n
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This Bruker AVIII 400 instrument provides capability for the study of a broad range nuclei for samples in the solid state. It has a range of probes that will accommodate 7 mm, 4 mm, or 2.5 mm rotors. <\/p>\n<\/div>\n\n\n\n

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Bruker Fourier 300 \u2013 Teal<\/em> \u2013 B300 TL<\/h3>\n\n\n\n
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This 300 MHz spectrometer, located in our synthesis teaching laboratory adjacent to Mass Spectrometry, HPLC and GC instruments, is dedicated to our undergraduate teaching program. It features a high-throughput 1<\/sup>H\/13<\/sup>C dual probe and 60 position SampleXpress sample changer which enables multiple data collections for each student in a teaching session.<\/p>\n<\/div>\n<\/div>\n\n\n\n

Varian VNMRS 500 \u2013 Ferret<\/em> \u2013 V500 B04<\/h3>\n\n\n\n
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This 3-channel 500 MHz instrument is the last in a long line of Varian NMR spectrometers in the department. The spectrometer is equipped with a wide range of probes that can access the frequency of almost any nucleus, with additional capabilities including triaxial gradients, LC flow, and H-X-Y tuning. <\/p>\n<\/div>\n\n\n\n

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Bruker AVIII 400 \u2013 Pink<\/em> \u2013 B400 B14<\/h3>\n\n\n\n
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This 400 MHz instrument is a core walk-up provider, It is fitted with a double resonance broadband probe which enables observation of 1<\/sup>H in addition to 19<\/sup>F or nuclei with frequencies from 31<\/sup>P to 15<\/sup>N. It has a sixty position BACS sample changer and is primarily used to run service samples in automation.<\/p>\n<\/div>\n<\/div>\n\n\n\n

Bruker AVIII 400 \u2013 Blue<\/em> \u2013 B400 B10<\/h3>\n\n\n\n
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This instrument is equipped with a double resonance broadband probe which enables observation of 1<\/sup>H and nuclei with frequencies from 31<\/sup>P to 15<\/sup>N, as well as 19<\/sup>F. It has a sixty position BACS sample changer and is primarily used to run service samples, reaction monitoring, and for NMR methodology research. The instrument may be booked for manual use by trained operators.<\/p>\n<\/div>\n\n\n\n

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Bruker DRX 300 \u2013 Ruby<\/em> \u2013 B300 B10<\/h3>\n\n\n\n
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The oldest instrument in our facility with a magnet dating back to 1996, the Bruker DRX 300 is equipped with a switched quattro nucleus probe for observation of 1<\/sup>H and 13<\/sup>C, 19<\/sup>F or 31<\/sup>P nuclei. The instrument provides ‘burst’ capacity for the walk-up service and is used for NMR methodology research projects, it has a sixty position BACS sample changer.<\/p>\n<\/div>\n<\/div>\n\n\n\n

Nanalysis 60PRO – Lime<\/em> – N60 TL<\/h3>\n\n\n\n
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This fully integrated and portable 1.4 T benchtop NMR spectrometer is equipped with a dual probe for collection of 1<\/sup>H and 31<\/sup>P spectra. It supports our undergraduate teaching program and vacation outreach activities. <\/p>\n<\/div>\n\n\n\n

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The NMR facility in the Department of Chemistry comprises of 11 NMR spectrometers at 300\u2013600 MHz including a 400 MHz solid state instrument and a 300 MHz instrument in the undergraduate teaching laboratory. Bruker AVIII HD 500 \u2013 Gold \u2013 B500 B14 This instrument is equipped with a nitrogen-cooled broadband Prodigy cryoprobe. It has a … <\/p>\n

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