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Setup List
Holder Status Name ExpNo Experiment User Time Title
1 Completed 2602191235-0-1-t19785ak 10 PROTON ug2023 00:01:58 90 degrees 17/02/2026 4-ep || 1H Experiment
2 Completed 2602191237-0-2-j42917hk 10 PROTON ug2023 00:01:58 Grp 23 HK || 1H Experiment
3 Completed 2602191305-0-3-a98524wr 10 PROTON ug2023 00:01:58 JMM, butrylaldehyde final product, 2.5 || 1H Experiment
4 Completed 2602191307-0-4-g14620tl 10 PROTON ug2023 00:01:58 WEEK 3 CRUDE || 1H Experiment
4 Completed 2602191307-0-4-g14620tl 11 P31CPD ug2023 00:00:54 WEEK 3 CRUDE || 31P{1H}, 1H Decoupled, 16 Scans
4 Completed 2602191307-0-4-g14620tl 12 P31 ug2023 00:01:37 WEEK 3 CRUDE || 31P Experiment, No Decoupling, 32 Scans
5 Completed 2602191307-0-5-g14620tl 10 PROTON ug2023 00:01:58 WEEK 3 CRUDE BIG (dilute) || 1H Experiment
5 Completed 2602191307-0-5-g14620tl 11 P31CPD ug2023 00:00:54 WEEK 3 CRUDE BIG (dilute) || 31P{1H}, 1H Decoupled, 16 Scans
5 Completed 2602191307-0-5-g14620tl 12 P31 ug2023 00:01:37 WEEK 3 CRUDE BIG (dilute) || 31P Experiment, No Decoupling, 32 Scans
6 Completed 2602191307-0-6-g14620tl 10 PROTON ug2023 00:01:58 WEEK 3 CRUDE SMALL (not dilute) || 1H Experiment
6 Completed 2602191307-0-6-g14620tl 11 P31CPD ug2023 00:00:54 WEEK 3 CRUDE SMALL (not dilute) || 31P{1H}, 1H Decoupled, 16 Scans
6 Completed 2602191307-0-6-g14620tl 12 P31 ug2023 00:01:37 WEEK 3 CRUDE SMALL (not dilute) || 31P Experiment, No Decoupling, 32 Scans
7 Completed 2602191325-0-7-f50609sc 10 PROTON ug2023 00:01:58 G38.S3.1.P || 1H Experiment
8 Completed 2602191325-0-8-f50609sc 10 PROTON ug2023 00:01:58 G38.S3.1.N || 1H Experiment
9 Completed 2602191327-0-9-v45005oc 10 C13CPD32 ug2023 00:02:12 OC Crude carbamate amine before column || 13C Experiment, 1H decoupled, 32 scans
9 Completed 2602191327-0-9-v45005oc 11 PROTON ug2023 00:01:58 OC Crude carbamate amine before column || 1H Experiment
10 Completed 2602191335-0-10-w32390no 10 PROTON ug2023 00:01:58 Epox prod || 1H Experiment
10 Completed 2602191335-0-10-w32390no 11 C13CPD32 ug2023 00:02:12 Epox prod || 13C Experiment, 1H decoupled, 32 scans
11 Submitted 2602191338-0-11-j77257is 10 PROTON ug2023 00:01:58 wk3 product after wash before column || 1H Experiment
11 Submitted 2602191338-0-11-j77257is 11 C13CPD32 ug2023 00:02:12 wk3 product after wash before column || 13C Experiment, 1H decoupled, 32 scans
12 Completed 2602191341-0-12-z82227gm 10 PROTON ug2023 00:01:58 Arthur || 1H Experiment
13 Submitted 2602191354-0-13-a98524wr 10 PROTON ug2023 00:01:58 JMM ,Week 3, Thursday, butryaldehyde:2.2, final product || 1H Experiment
14 Completed 2602191349-0-14-c68402hw 10 PROTON ug2023 00:01:58 Urea B second || 1H Experiment
14 Completed 2602191349-0-14-c68402hw 11 C13CPD32 ug2023 00:02:12 Urea B second || 13C Experiment, 1H decoupled, 32 scans
15 Completed 2602191349-0-15-c68402hw 10 PROTON ug2023 00:01:58 Urea B second filtrate || 1H Experiment
16 Completed 2602191349-0-16-c68402hw 10 PROTON ug2023 00:01:58 Urea B Full || 1H Experiment
16 Completed 2602191349-0-16-c68402hw 11 C13CPD32 ug2023 00:02:12 Urea B Full || 13C Experiment, 1H decoupled, 32 scans
16 Completed 2602191349-0-16-c68402hw 12 COSYGPSW ug2023 00:05:34 Urea B Full || COSY
16 Completed 2602191349-0-16-c68402hw 13 HSQCEDETGP ug2023 00:14:34 Urea B Full || 1-bond 1H-13C correlation with CH/CH3 up and CH2 down
16 Running 2602191349-0-16-c68402hw 14 HMBCLPND ug2023 02:24:07 Urea B Full || Long range 1H-13C correlation
17 Submitted 2602191354-0-17-a98524wr 10 PROTON ug2023 00:01:58 Jerry, Week 3, Thursday, Isobutyraldehyde 1:2.2 (product solidified so took a sample) || 1H Experiment
18 Submitted 2602191354-0-18-a98524wr 10 PROTON ug2023 00:01:58 Jerry, Week 3, Thursday, Isobutyraldehyde 1:2.5 with basic alumina final product || 1H Experiment
19 Submitted 2602191357-0-19-w75830yw 10 PROTON ug2023 00:01:58 bromine pure OMe || 1H Experiment
19 Submitted 2602191357-0-19-w75830yw 11 C13CPD32 ug2023 00:02:12 bromine pure OMe || 13C Experiment, 1H decoupled, 32 scans
20 Submitted 2602191408-0-20-j80847ja 10 PROTON ug2023 00:01:58 lee terpinene post column(18-21) || 1H Experiment
20 Submitted 2602191408-0-20-j80847ja 11 C13CPD32 ug2023 00:02:12 lee terpinene post column(18-21) || 13C Experiment, 1H decoupled, 32 scans
20 Submitted 2602191408-0-20-j80847ja 12 COSYGPSW ug2023 00:05:34 lee terpinene post column(18-21) || COSY
21 Submitted 2602191408-0-21-j80847ja 10 PROTON ug2023 00:01:58 lee terpinene post column(25-27) || 1H Experiment
21 Submitted 2602191408-0-21-j80847ja 11 C13CPD32 ug2023 00:02:12 lee terpinene post column(25-27) || 13C Experiment, 1H decoupled, 32 scans
21 Submitted 2602191408-0-21-j80847ja 12 COSYGPSW ug2023 00:05:34 lee terpinene post column(25-27) || COSY
22 Submitted 2602191448-0-22-a98524wr 10 PROTON ug2023 00:01:58 Will Week 3 Thursday Step 1 Reaction 1 trimethylacetaldehyde 1:1.1 || 1H Experiment
22 Submitted 2602191448-0-22-a98524wr 11 C13CPD32 ug2023 00:02:12 Will Week 3 Thursday Step 1 Reaction 1 trimethylacetaldehyde 1:1.1 || 13C Experiment, 1H decoupled, 32 scans
23 Submitted 2602191448-0-23-a98524wr 10 PROTON ug2023 00:01:58 Will Week 3 Thursday Step 1 Reaction 2 Trimethylacetaldehyde 1:2.2 || 1H Experiment
23 Submitted 2602191448-0-23-a98524wr 11 C13CPD32 ug2023 00:02:12 Will Week 3 Thursday Step 1 Reaction 2 Trimethylacetaldehyde 1:2.2 || 13C Experiment, 1H decoupled, 32 scans
24 Submitted 2602191448-0-24-a98524wr 10 PROTON ug2023 00:01:58 Will Week 3 Thursday Step 1 Reaction 3 Butyraldehyde 1:2.2 (50 mmol scale up) || 1H Experiment
24 Submitted 2602191448-0-24-a98524wr 11 C13CPD32 ug2023 00:02:12 Will Week 3 Thursday Step 1 Reaction 3 Butyraldehyde 1:2.2 (50 mmol scale up) || 13C Experiment, 1H decoupled, 32 scans
25 Submitted 2602191503-0-25-j42917hk 10 PROTON ug2023 00:01:58 Grp 23 E2 HK || 1H Experiment
26 Submitted 2602191511-0-26-c22796za 10 PROTON ug2023 00:01:58 SM of nitroaniline || 1H Experiment
26 Submitted 2602191511-0-26-c22796za 11 C13CPD32 ug2023 00:02:12 SM of nitroaniline || 13C Experiment, 1H decoupled, 32 scans
27 Submitted 2602191451-0-27-c68704nm 10 PROTON ug2023 00:01:58 Dini_Part2_Tube9-12 || 1H Experiment
27 Submitted 2602191451-0-27-c68704nm 11 C13CPD32 ug2023 00:02:12 Dini_Part2_Tube9-12 || 13C Experiment, 1H decoupled, 32 scans
28 Submitted 2602191454-0-28-m20809op 10 PROTON ug2023 00:01:58 Sodium sulphate product || 1H Experiment
29 Submitted 2602191457-0-29-c68704nm 10 PROTON ug2023 00:01:58 Dini_Part2_Tube6 || 1H Experiment
29 Submitted 2602191457-0-29-c68704nm 11 C13CPD32 ug2023 00:02:12 Dini_Part2_Tube6 || 13C Experiment, 1H decoupled, 32 scans
30 Completed 2602191047-0-30-z73813ns 10 PROTON ug2023 00:01:58 NS Urea D R2 1H 13C || 1H Experiment
30 Submitted 2602191047-0-30-z73813ns 11 C13CPD32 ug2023 00:02:12 NS Urea D R2 1H 13C || 13C Experiment, 1H decoupled, 32 scans
31 Submitted 2602191631-0-31-q84930bb 10 PROTON ug2023 00:01:58 BBW F19 O2 || 1H Experiment
31 Submitted 2602191631-0-31-q84930bb 11 C13CPD ug2023 01:06:44 BBW F19 O2 || 13C Experiment, 1H decoupled, 128 scans
31 Submitted 2602191631-0-31-q84930bb 12 F19 ug2023 00:00:39 BBW F19 O2 || 19F Experiment
32 Completed 2602191058-0-32-a59382yh 10 PROTON ug2023 00:01:58 4aminobenzonitriletoluene || 1H Experiment
32 Completed 2602191058-0-32-a59382yh 11 C13CPD32 ug2023 00:02:12 4aminobenzonitriletoluene || 13C Experiment, 1H decoupled, 32 scans
33 Submitted 2602191457-0-33-c68704nm 10 PROTON ug2023 00:01:58 Dini_Part2_Tube7-8 || 1H Experiment
33 Submitted 2602191457-0-33-c68704nm 11 C13CPD32 ug2023 00:02:12 Dini_Part2_Tube7-8 || 13C Experiment, 1H decoupled, 32 scans
34 Completed 2602191100-0-34-s81742yz 11 C13CPD ug2023 01:06:44 W2NHCproductI || 13C Experiment, 1H decoupled, 128 scans
34 Completed 2602191100-0-34-s81742yz 12 F19 ug2023 00:00:39 W2NHCproductI || 19F Experiment
35 Submitted 2602191509-0-35-z34413sw 10 C13CPD32 ug2023 00:02:12 G14-OMe-alcohol || 13C Experiment, 1H decoupled, 32 scans
35 Submitted 2602191509-0-35-z34413sw 11 C13CPD ug2023 01:06:44 G14-OMe-alcohol || 13C Experiment, 1H decoupled, 128 scans
36 Submitted 2602191509-0-36-z34413sw 10 C13CPD32 ug2023 00:02:12 G14-OMe-Fin || 13C Experiment, 1H decoupled, 32 scans
36 Submitted 2602191509-0-36-z34413sw 11 C13CPD ug2023 01:06:44 G14-OMe-Fin || 13C Experiment, 1H decoupled, 128 scans
37 Submitted 2602191509-0-37-z34413sw 10 C13CPD32 ug2023 00:02:12 G14-CF3-start || 13C Experiment, 1H decoupled, 32 scans
37 Submitted 2602191509-0-37-z34413sw 11 C13CPD ug2023 01:06:44 G14-CF3-start || 13C Experiment, 1H decoupled, 128 scans
37 Submitted 2602191509-0-37-z34413sw 12 F19 ug2023 00:00:39 G14-CF3-start || 19F Experiment
38 Submitted 2602191509-0-38-z34413sw 10 C13CPD32 ug2023 00:02:12 G14-NMe2-start || 13C Experiment, 1H decoupled, 32 scans
38 Submitted 2602191509-0-38-z34413sw 11 C13CPD ug2023 01:06:44 G14-NMe2-start || 13C Experiment, 1H decoupled, 128 scans
39 Submitted 2602191514-0-39-p00146sh 10 PROTON ug2023 00:01:58 NFSI starting material G30 || 1H Experiment
39 Submitted 2602191514-0-39-p00146sh 11 C13CPD32 ug2023 00:02:12 NFSI starting material G30 || 13C Experiment, 1H decoupled, 32 scans
39 Submitted 2602191514-0-39-p00146sh 12 F19 ug2023 00:00:39 NFSI starting material G30 || 19F Experiment
40 Submitted 2602191514-0-40-p00146sh 10 PROTON ug2023 00:01:58 Shoujun Crude Catalyst Ligand G30 || 1H Experiment
40 Submitted 2602191514-0-40-p00146sh 11 C13CPD32 ug2023 00:02:12 Shoujun Crude Catalyst Ligand G30 || 13C Experiment, 1H decoupled, 32 scans
41 Submitted 2602191516-0-41-m00673hs 10 PROTON ug2023 00:01:58 Proline 10 || 1H Experiment
42 Submitted 2602191516-0-42-m00673hs 10 PROTON ug2023 00:01:58 Proline 20 || 1H Experiment
43 Submitted 2602191525-0-43-n77009rc 10 PROTON ug2023 00:01:58 Clover Glucose || 1H Experiment
44 Submitted 2602191525-0-44-n77009rc 10 PROTON ug2023 00:01:58 Clover HMF || 1H Experiment
45 Submitted 2602191119-0-45-t16779zc 11 C13CPD32 ug2023 00:02:12 final p1 || 13C Experiment, 1H decoupled, 32 scans
46 Submitted 2602191133-0-46-d34693sa 11 C13CPD32 ug2023 00:02:12 Intermediate from 4-methylaniline NHC || 13C Experiment, 1H decoupled, 32 scans
47 Submitted 2602191137-0-47-q45256xh 11 C13CPD32 ug2023 00:02:12 week1 OAc || 13C Experiment, 1H decoupled, 32 scans
48 Submitted 2602191526-0-48-m00673hs 10 PROTON ug2023 00:01:58 Proline 30 || 1H Experiment
49 Submitted 2602191147-0-49-g17166lh 11 C13CPD32 ug2023 00:02:12 lee 2nd layer gamma terpinene || 13C Experiment, 1H decoupled, 32 scans
50 Submitted 2602191526-0-50-m00673hs 10 PROTON ug2023 00:01:58 Proline 40 || 1H Experiment
51 Submitted 2602191526-0-51-m00673hs 10 PROTON ug2023 00:01:58 Proline 50 || 1H Experiment
52 Submitted 2602191529-0-52-z91447bd 10 PROTON ug2023 00:01:58 Purified Product 2 || 1H Experiment
52 Submitted 2602191529-0-52-z91447bd 11 C13CPD32 ug2023 00:02:12 Purified Product 2 || 13C Experiment, 1H decoupled, 32 scans
53 Submitted 2602191150-0-53-g17166lh 11 C13CPD32 ug2023 00:02:12 Jinny gamma terpinene (ben) || 13C Experiment, 1H decoupled, 32 scans
54 Completed 2602191150-0-54-g17166lh 10 PROTON ug2023 00:01:58 Jinny bottom layer || 1H Experiment
54 Submitted 2602191150-0-54-g17166lh 11 C13CPD32 ug2023 00:02:12 Jinny bottom layer || 13C Experiment, 1H decoupled, 32 scans
54 Completed 2602191150-0-54-g17166lh 12 COSYGPSW ug2023 00:05:34 Jinny bottom layer || COSY
55 Completed 2602191158-0-55-d96985hs 10 PROTON ug2023 00:01:58 HSWeek3Thur b1 || 1H Experiment
55 Completed 2602191158-0-55-d96985hs 11 C13CPD32 ug2023 00:02:12 HSWeek3Thur b1 || 13C Experiment, 1H decoupled, 32 scans
56 Completed 2602191158-0-56-d96985hs 10 PROTON ug2023 00:01:58 HSWeek3Thur i1 || 1H Experiment
56 Completed 2602191158-0-56-d96985hs 11 C13CPD32 ug2023 00:02:12 HSWeek3Thur i1 || 13C Experiment, 1H decoupled, 32 scans
57 Completed 2602191158-0-57-a98524wr 10 PROTON ug2023 00:01:58 JMM, butryaldehyde:2.2 30 minutes || 1H Experiment
58 Completed 2602191207-0-58-a98524wr 10 PROTON ug2023 00:01:58 JMM, Butryaldehyde:2.2 40 minutes || 1H Experiment
59 Completed 2602191210-0-59-a59382yh 10 PROTON ug2023 00:01:58 Anilineintermediatetoluene || 1H Experiment
59 Completed 2602191210-0-59-a59382yh 11 C13CPD32 ug2023 00:02:12 Anilineintermediatetoluene || 13C Experiment, 1H decoupled, 32 scans
60 Completed 2602191214-0-60-d96985hs 10 PROTON ug2023 00:01:58 HSWeek3Thurs B2 || 1H Experiment
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
16 20:43:54 2602191349-0-16-c68402hw 14 HMBCLPND ug2023 - + - - - - - Urea B Full || Long range 1H-13C correlation
16 20:27:59 2602191349-0-16-c68402hw 13 HSQCEDETGP ug2023 - + - - - + + Urea B Full || 1-bond 1H-13C correlation with CH/CH3 up and CH2 down
16 20:21:51 2602191349-0-16-c68402hw 12 COSYGPSW ug2023 - + - - - + + Urea B Full || COSY
16 20:18:50 2602191349-0-16-c68402hw 11 C13CPD32 ug2023 - + - - - + + Urea B Full || 13C Experiment, 1H decoupled, 32 scans
16 20:13:39 2602191349-0-16-c68402hw 10 PROTON ug2023 + + - + + + + Urea B Full || 1H Experiment
15 20:08:26 2602191349-0-15-c68402hw 10 PROTON ug2023 + + - + + + + Urea B second filtrate || 1H Experiment
14 20:05:30 2602191349-0-14-c68402hw 11 C13CPD32 ug2023 - + - - - + + Urea B second || 13C Experiment, 1H decoupled, 32 scans
14 20:00:14 2602191349-0-14-c68402hw 10 PROTON ug2023 + + - + + + + Urea B second || 1H Experiment
12 19:54:59 2602191341-0-12-z82227gm 10 PROTON ug2023 + + - + + + + Arthur || 1H Experiment
10 19:52:00 2602191335-0-10-w32390no 11 C13CPD32 ug2023 - + - - - + + Epox prod || 13C Experiment, 1H decoupled, 32 scans
10 19:45:51 2602191335-0-10-w32390no 10 PROTON ug2023 + + - + + + + Epox prod || 1H Experiment
9 19:43:06 2602191327-0-9-v45005oc 11 PROTON ug2023 - + - - - + + OC Crude carbamate amine before column || 1H Experiment
9 19:36:46 2602191327-0-9-v45005oc 10 C13CPD32 ug2023 + + - + + + + OC Crude carbamate amine before column || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602191327-0-9-v45005oc/10/pdata/1/peaks No peaks found in the specified range.
8 19:30:35 2602191325-0-8-f50609sc 10 PROTON ug2023 + + - + + + + G38.S3.1.N || 1H Experiment
7 19:22:44 2602191325-0-7-f50609sc 10 PROTON ug2023 + + - + + + + G38.S3.1.P || 1H Experiment
6 19:20:40 2602191307-0-6-g14620tl 12 P31 ug2023 - + - - - + + WEEK 3 CRUDE SMALL (not dilute) || 31P Experiment, No Decoupling, 32 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'MeOD' SR is set to 0.0
6 19:19:00 2602191307-0-6-g14620tl 11 P31CPD ug2023 - + - - - + + WEEK 3 CRUDE SMALL (not dilute) || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'MeOD' SR is set to 0.0
6 19:13:44 2602191307-0-6-g14620tl 10 PROTON ug2023 + + - + + + + WEEK 3 CRUDE SMALL (not dilute) || 1H Experiment
5 19:11:39 2602191307-0-5-g14620tl 12 P31 ug2023 - + - - - + + WEEK 3 CRUDE BIG (dilute) || 31P Experiment, No Decoupling, 32 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'MeOD' SR is set to 0.0
5 19:09:59 2602191307-0-5-g14620tl 11 P31CPD ug2023 - + - - - + + WEEK 3 CRUDE BIG (dilute) || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'MeOD' SR is set to 0.0
5 19:04:36 2602191307-0-5-g14620tl 10 PROTON ug2023 + + - + + + + WEEK 3 CRUDE BIG (dilute) || 1H Experiment
4 19:02:31 2602191307-0-4-g14620tl 12 P31 ug2023 - + - - - + + WEEK 3 CRUDE || 31P Experiment, No Decoupling, 32 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0; pp: Cannot find any peak for scaling in /mnt/nmrdata/nomad/data/ug2023/nmr/2602191307-0-4-g14620tl/12/pdata/1/peaks
4 19:00:29 2602191307-0-4-g14620tl 11 P31CPD ug2023 - + - - - + + WEEK 3 CRUDE || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0
4 18:53:52 2602191307-0-4-g14620tl 10 PROTON ug2023 + + - + + + + WEEK 3 CRUDE || 1H Experiment
3 18:44:50 2602191305-0-3-a98524wr 10 PROTON ug2023 + + - + + + + JMM, butrylaldehyde final product, 2.5 || 1H Experiment
32 18:41:57 2602191058-0-32-a59382yh 11 C13CPD32 ug2023 - + - - - + + 4aminobenzonitriletoluene || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602191058-0-32-a59382yh/11/pdata/1/peaks No peaks found in the specified range.
32 18:34:35 2602191058-0-32-a59382yh 10 PROTON ug2023 + + - + + + + 4aminobenzonitriletoluene || 1H Experiment
2 18:27:31 2602191237-0-2-j42917hk 10 PROTON ug2023 + + - + + + + Grp 23 HK || 1H Experiment
1 18:18:36 2602191235-0-1-t19785ak 10 PROTON ug2023 + + - + + + + 90 degrees 17/02/2026 4-ep || 1H Experiment
60 18:12:24 2602191214-0-60-d96985hs 10 PROTON ug2023 + + - + + + + HSWeek3Thurs B2 || 1H Experiment
59 18:09:31 2602191210-0-59-a59382yh 11 C13CPD32 ug2023 - + - - - + + Anilineintermediatetoluene || 13C Experiment, 1H decoupled, 32 scans
59 18:01:35 2602191210-0-59-a59382yh 10 PROTON ug2023 + + - + + + + Anilineintermediatetoluene || 1H Experiment
58 17:54:14 2602191207-0-58-a98524wr 10 PROTON ug2023 + + - + + + + JMM, Butryaldehyde:2.2 40 minutes || 1H Experiment
55 17:51:21 2602191158-0-55-d96985hs 11 C13CPD32 ug2023 - + - - - + + HSWeek3Thur b1 || 13C Experiment, 1H decoupled, 32 scans
55 17:43:50 2602191158-0-55-d96985hs 10 PROTON ug2023 + + - + + + + HSWeek3Thur b1 || 1H Experiment
56 17:40:11 2602191158-0-56-d96985hs 11 C13CPD32 ug2023 - + - - - + + HSWeek3Thur i1 || 13C Experiment, 1H decoupled, 32 scans
56 17:32:14 2602191158-0-56-d96985hs 10 PROTON ug2023 + + - + + + + HSWeek3Thur i1 || 1H Experiment
57 17:25:38 2602191158-0-57-a98524wr 10 PROTON ug2023 + + - + + + + JMM, butryaldehyde:2.2 30 minutes || 1H Experiment
34 17:23:59 2602191100-0-34-s81742yz 12 F19 ug2023 - + - - - + + W2NHCproductI || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
34 16:13:06 2602191100-0-34-s81742yz 11 C13CPD ug2023 + + - + + + + W2NHCproductI || 13C Experiment, 1H decoupled, 128 scans
31 16:09:52 2602191058-0-31-a59382yh 11 C13CPD32 ug2023 - + - - - + + 4amiinobenzonitrileethylacetate || 13C Experiment, 1H decoupled, 32 scans
31 16:01:28 2602191058-0-31-a59382yh 10 PROTON ug2023 + + - + + + + 4amiinobenzonitrileethylacetate || 1H Experiment
30 15:53:07 2602191047-0-30-z73813ns 10 PROTON ug2023 + + - + + + + NS Urea D R2 1H 13C || 1H Experiment
54 15:47:00 2602191150-0-54-g17166lh 12 COSYGPSW ug2023 - + - - - + + Jinny bottom layer || COSY
54 15:36:14 2602191150-0-54-g17166lh 10 PROTON ug2023 + + - + + + + Jinny bottom layer || 1H Experiment
53 15:30:06 2602191150-0-53-g17166lh 12 COSYGPSW ug2023 - + - - - + + Jinny gamma terpinene (ben) || COSY
53 15:23:03 2602191150-0-53-g17166lh 10 PROTON ug2023 + + - + + + + Jinny gamma terpinene (ben) || 1H Experiment
52 15:16:20 2602191149-0-52-z34413sw 10 PROTON ug2023 + + - + + + + G14-CDCl3 || 1H Experiment
51 15:07:49 2602191149-0-51-z34413sw 10 PROTON ug2023 + + - + + + + G14-OMe-triflro-acetate || 1H Experiment
50 15:01:08 2602191147-0-50-a98524wr 10 PROTON ug2023 + + - + + + + JMM, butryaldehyde:2.2 20 mins || 1H Experiment
49 14:54:58 2602191147-0-49-g17166lh 12 COSYGPSW ug2023 - + - - - + + lee 2nd layer gamma terpinene || COSY
49 14:48:12 2602191147-0-49-g17166lh 10 PROTON ug2023 + + - + + + + lee 2nd layer gamma terpinene || 1H Experiment
48 14:40:38 2602191137-0-48-a98524wr 10 PROTON ug2023 + + - + + + + JMM, butryaldehyde:2.2 10 minutes || 1H Experiment
47 14:34:30 2602191137-0-47-q45256xh 10 PROTON ug2023 + + - + + + + week1 OAc || 1H Experiment
46 14:28:17 2602191133-0-46-d34693sa 10 PROTON ug2023 + + - + + + + Intermediate from 4-methylaniline NHC || 1H Experiment
45 14:21:35 2602191119-0-45-t16779zc 10 PROTON ug2023 + + - + + + + final p1 || 1H Experiment
44 14:15:17 2602191115-0-44-n77009rc 10 PROTON ug2023 + + - + + + + Manuka glucose || 1H Experiment
46 14:14:32 2602191133-0-46-d34693sa 10 PROTON ug2023 x - - - - - - Intermediate from 4-methylaniline NHC || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
45 14:14:29 2602191119-0-45-t16779zc 10 PROTON ug2023 x - - - - - - final p1 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
44 14:14:13 2602191115-0-44-n77009rc 10 PROTON ug2023 x - - - - - - Manuka glucose || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Inconsistent Inputs detected by Controller, please check light barriers. SMCB input word: 0x00021B43
43 14:08:25 2602191115-0-43-n77009rc 10 PROTON ug2023 + + - + + + + Manuka HMF || 1H Experiment
45 13:58:27 2602191119-0-45-t16779zc 10 PROTON ug2023 x - - - - - - final p1 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
44 13:58:24 2602191115-0-44-n77009rc 10 PROTON ug2023 x - - - - - - Manuka glucose || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
43 13:58:09 2602191115-0-43-n77009rc 10 PROTON ug2023 x - - - - - - Manuka HMF || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Inconsistent Inputs detected by Controller, please check light barriers. SMCB input word: 0x00022B43
42 13:53:06 2602191115-0-42-n77009rc 10 PROTON ug2023 + + - + + + + Manuka Proline || 1H Experiment
41 13:47:26 2602191115-0-41-n77009rc 10 PROTON ug2023 + + - + + + + Blank || 1H Experiment
40 13:41:24 2602191115-0-40-n77009rc 10 PROTON ug2023 + + - + + + + Clover 1 || 1H Experiment
39 13:35:49 2602191114-0-39-s04936gr 10 PROTON ug2023 + + - + + + + blank-all || 1H Experiment
38 13:30:20 2602191114-0-38-s04936gr 10 PROTON ug2023 + + - + + + + wf-proline || 1H Experiment
37 13:24:19 2602191114-0-37-s04936gr 10 PROTON ug2023 + + - + + + + wf-hmf || 1H Experiment
36 13:19:18 2602191114-0-36-s04936gr 10 PROTON ug2023 + + - + + + + wf-glu || 1H Experiment
35 13:13:16 2602191114-0-35-s04936gr 10 PROTON ug2023 + + - + + + + manuka4 || 1H Experiment
34 13:06:14 2602191100-0-34-s81742yz 10 PROTON ug2023 + + - + + + + W2NHCproductI || 1H Experiment
33 13:03:01 2602191059-0-33-s05774bb 11 C13CPD32 ug2023 - + - - - + + BB R=Cl scale up || 13C Experiment, 1H decoupled, 32 scans
33 12:55:12 2602191059-0-33-s05774bb 10 PROTON ug2023 + + - + + + + BB R=Cl scale up || 1H Experiment
32 12:45:14 2602191058-0-32-a59382yh 10 PROTON ug2023 x - - - - - - 4aminobenzonitriletoluene || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
31 12:45:11 2602191058-0-31-a59382yh 10 PROTON ug2023 x - - - - - - 4amiinobenzonitrileethylacetate || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
30 12:45:06 2602191047-0-30-z73813ns 10 PROTON ug2023 x - - - - - - NS Urea D R2 1H 13C || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Compressed air pressure ( 125232 Pa) out of range. Aborting command.
29 12:42:13 2602191043-0-29-c22796za 11 C13CPD32 ug2023 - + - - - + + Ethyl acetate of nitro before BHF4 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602191043-0-29-c22796za/11/pdata/1/peaks No peaks found in the specified range.
29 12:33:45 2602191043-0-29-c22796za 10 PROTON ug2023 + + - + + + + Ethyl acetate of nitro before BHF4 || 1H Experiment
28 12:30:54 2602191043-0-28-c22796za 11 C13CPD32 ug2023 - + - - - + + Toluene of nitro, before BHF4 || 13C Experiment, 1H decoupled, 32 scans
28 12:21:58 2602191043-0-28-c22796za 10 PROTON ug2023 + + - + + + + Toluene of nitro, before BHF4 || 1H Experiment
27 12:15:48 2602191042-0-27-e96670hy 10 PROTON ug2023 + + - + + + + PMBCl || 1H Experiment
26 12:12:55 2602191037-0-26-z91447bd 11 C13CPD32 ug2023 - + - - - + + Crude product 2 || 13C Experiment, 1H decoupled, 32 scans
26 12:07:12 2602191037-0-26-z91447bd 10 PROTON ug2023 + + - + + + + Crude product 2 || 1H Experiment
25 12:03:30 2602191037-0-25-z91447bd 11 C13CPD32 ug2023 - + - - - + + Impurity 1 || 13C Experiment, 1H decoupled, 32 scans
25 11:55:49 2602191037-0-25-z91447bd 10 PROTON ug2023 + + - + + + + Impurity 1 || 1H Experiment
24 11:46:56 2602191026-0-24-z34413sw 10 PROTON ug2023 + + - + + + + G14-CDCl3 || 1H Experiment
15 11:42:25 2602191026-0-15-z34413sw 10 F19 ug2023 + + - + + + + G14-CF3-FNMR || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
14 11:40:41 2602191021-0-14-p00146sh 12 F19 ug2023 - + - - - + + Sam Fluoroamide Crude Product G30 || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
14 11:37:48 2602191021-0-14-p00146sh 11 C13CPD32 ug2023 - + - - - + + Sam Fluoroamide Crude Product G30 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602191021-0-14-p00146sh/11/pdata/1/peaks No peaks found in the specified range.
14 11:31:35 2602191021-0-14-p00146sh 10 PROTON ug2023 + + - + + + + Sam Fluoroamide Crude Product G30 || 1H Experiment
13 11:23:05 2602191015-0-13-t69807al 10 PROTON ug2023 + + - + + + + Urea A.2 || 1H Experiment
11 11:20:11 2602191014-0-11-b93379br 11 C13CPD32 ug2023 - + - - - + + Terpinene Before Rotary Evap || 13C Experiment, 1H decoupled, 32 scans
11 11:11:46 2602191014-0-11-b93379br 10 PROTON ug2023 + + - + + + + Terpinene Before Rotary Evap || 1H Experiment
10 11:08:53 2602191014-0-10-b93379br 11 C13CPD32 ug2023 - + - - - + + Limonene Before Rotary Evap || 13C Experiment, 1H decoupled, 32 scans
10 11:02:47 2602191014-0-10-b93379br 10 PROTON ug2023 + + - + + + + Limonene Before Rotary Evap || 1H Experiment
9 10:56:41 2602191015-0-9-j80847ja 12 COSYGPSW ug2023 - + - - - + + lee terpinene (precolumn 2) || COSY
9 10:53:48 2602191015-0-9-j80847ja 11 C13CPD32 ug2023 - + - - - + + lee terpinene (precolumn 2) || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602191015-0-9-j80847ja/11/pdata/1/peaks No peaks found in the specified range.
9 10:45:22 2602191015-0-9-j80847ja 10 PROTON ug2023 + + - + + + + lee terpinene (precolumn 2) || 1H Experiment
8 10:42:27 2602191015-0-8-j80847ja 11 C13CPD32 ug2023 - + - - - + + jinny myrcene (precolumn) || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602191015-0-8-j80847ja/11/pdata/1/peaks No peaks found in the specified range.
8 10:36:12 2602191015-0-8-j80847ja 10 PROTON ug2023 + + - + + + + jinny myrcene (precolumn) || 1H Experiment
7 10:32:32 2602191015-0-7-j80847ja 11 C13CPD32 ug2023 - + - - - + + jood myrcene(precolumn) || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602191015-0-7-j80847ja/11/pdata/1/peaks No peaks found in the specified range.
7 10:24:29 2602191015-0-7-j80847ja 10 PROTON ug2023 + + - + + + + jood myrcene(precolumn) || 1H Experiment
6 10:22:37 2602191012-0-6-t29189mm 12 F19 ug2023 - + - - - + + alcohol g || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
6 10:19:45 2602191012-0-6-t29189mm 11 C13CPD32 ug2023 - + - - - + + alcohol g || 13C Experiment, 1H decoupled, 32 scans
6 10:12:40 2602191012-0-6-t29189mm 10 PROTON ug2023 + + - + + + + alcohol g || 1H Experiment
12 12:23:09 2602171530-0-12-j13260ec 11 C13CPD32 ug2024 + + - + + + + EXP_W || 13C Experiment, 1H decoupled, 32 scans
18 12:15:15 2602181033-0-18-p46928my 10 PROTON ug2024 + + - + + + + Mohammed Yousef || 1H Experiment
4 12:12:23 2602181132-0-4-n00101ja 11 C13CPD32 ug2024 - + - - - + + Joanne Alghanem EXP14 || 13C Experiment, 1H decoupled, 32 scans
4 12:04:48 2602181132-0-4-n00101ja 10 PROTON ug2024 + + - + + + + Joanne Alghanem EXP14 || 1H Experiment
3 12:01:55 2602181104-0-3-j39140yc 11 C13CPD32 ug2024 - + - - - + + yuzhu_c_nmr || 13C Experiment, 1H decoupled, 32 scans
3 11:55:40 2602181104-0-3-j39140yc 10 PROTON ug2024 + + - + + + + yuzhu_c_nmr || 1H Experiment
2 11:49:34 2602181104-0-2-m33708xb 10 PROTON ug2024 + + - + + + + Exp.14 xuanqi bao || 1H Experiment
1 11:46:38 2602181108-0-1-n59525eg 11 C13CPD32 ug2024 - + - - - + + Exp 14 nmr || 13C Experiment, 1H decoupled, 32 scans
1 11:38:16 2602181108-0-1-n59525eg 10 PROTON ug2024 + + - + + + + Exp 14 nmr || 1H Experiment
23 11:31:10 2602181047-0-23-t12661yh 10 PROTON ug2024 + + - + + + + exp14 YH || 1H Experiment
22 11:25:00 2602181042-0-22-g17124ko 12 COSYGPSW ug2024 - + - - - + + 4-methoxy-4'-acetobiphenyl || COSY
22 11:21:50 2602181042-0-22-g17124ko 11 C13CPD32 ug2024 - + - - - + + 4-methoxy-4'-acetobiphenyl || 13C Experiment, 1H decoupled, 32 scans
22 11:13:47 2602181042-0-22-g17124ko 10 PROTON ug2024 + + - + + + + 4-methoxy-4'-acetobiphenyl || 1H Experiment
21 11:07:39 2602181040-0-21-e63518pk 10 PROTON ug2024 + + - + + + + PK-exp14 || 1H Experiment
20 11:01:23 2602181037-0-20-w37202lb 10 PROTON ug2024 + + - + + + + LilyB14 || 1H Experiment
19 10:54:37 2602181034-0-19-y96588sl 10 PROTON ug2024 + + - + + + + Exp14SL || 1H Experiment
17 10:47:27 2602181023-0-17-m97120dp 10 PROTON ug2024 + + - + + + + D.P X14 || 1H Experiment
16 10:40:50 2602181022-0-16-q95876fc 10 PROTON ug2024 + + - + + + + frankie exp 4 || 1H Experiment
19 10:38:11 2602181034-0-19-y96588sl 10 PROTON ug2024 x - - - - - - Exp14SL || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
17 10:38:08 2602181023-0-17-m97120dp 10 PROTON ug2024 x - - - - - - D.P X14 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
16 10:37:53 2602181022-0-16-q95876fc 10 PROTON ug2024 x - - - - - - frankie exp 4 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Inconsistent Inputs detected by Controller, please check light barriers. SMCB input word: 0x00011B43
15 10:31:45 2602181018-0-15-y98366wr 12 COSYGPSW ug2024 - + - - - + + WR X14 || COSY
15 10:28:45 2602181018-0-15-y98366wr 11 C13CPD32 ug2024 - + - - - + + WR X14 || 13C Experiment, 1H decoupled, 32 scans
15 10:20:13 2602181018-0-15-y98366wr 10 PROTON ug2024 + + - + + + + WR X14 || 1H Experiment
12 10:13:56 2602171530-0-12-j13260ec 10 PROTON ug2024 + + - + + + + EXP_W || 1H Experiment
11 10:11:11 2602171528-0-11-j13260ec 11 PROTON ug2024 - + - - - + + EXP14_C || 1H Experiment
11 10:04:22 2602171528-0-11-j13260ec 10 C13CPD32 ug2024 + + - + + + + EXP14_C || 13C Experiment, 1H decoupled, 32 scans
10 16:52:36 2602171524-0-10-y44022jb 11 C13CPD32 ug2024 - + - - - + + JB nmrex4 || 13C Experiment, 1H decoupled, 32 scans
10 16:44:01 2602171524-0-10-y44022jb 10 PROTON ug2024 + + - + + + + JB nmrex4 || 1H Experiment
9 16:37:50 2602171523-0-9-n42665oc 12 COSYGPSW ug2024 - + - - - + + Exp 4 product R || COSY
9 16:34:58 2602171523-0-9-n42665oc 11 C13CPD32 ug2024 - + - - - + + Exp 4 product R || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602171523-0-9-n42665oc/11/pdata/1/peaks No peaks found in the specified range.
9 16:28:15 2602171523-0-9-n42665oc 10 PROTON ug2024 + + - + + + + Exp 4 product R || 1H Experiment
8 16:22:10 2602171518-0-8-x37791lj 12 COSYGPSW ug2024 - + - - - + + NMR experiment 4 || COSY
8 16:18:22 2602171518-0-8-x37791lj 11 C13CPD32 ug2024 - x - - - + + NMR experiment 4 || 13C Experiment, 1H decoupled, 32 scans log_err:
In experiment: 2602171518-0-8-x37791lj 11 1 /mnt/nmrdata/nomad/data/ug2024/nmr
(Parameter Set = 'C13CPD32')

Exception in drucontr-TRX2:  FOOTER: Error from DRX:
Acquisition has been started too early after changing RG ->Experiment aborted by TRX2!

In experiment: 2602171518-0-8-x37791lj 11 1 /mnt/nmrdata/nomad/data/ug2024/nmr
(Parameter Set = 'C13CPD32')

Exception in drucontr-TRX1:  FOOTER: Error from DRX:
Acquisition has been started too early after changing RG ->Experiment aborted by TRX1!
, Wobbling error. Details:, ATM Failed
8 16:10:44 2602171518-0-8-x37791lj 10 PROTON ug2024 + + - + + + + NMR experiment 4 || 1H Experiment
7 16:04:30 2602171514-0-7-n42665oc 12 COSYGPSW ug2024 - + - - - + + Exp 4 Product || COSY
7 16:01:32 2602171514-0-7-n42665oc 11 C13CPD32 ug2024 - + - - - + + Exp 4 Product || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602171514-0-7-n42665oc/11/pdata/1/peaks No peaks found in the specified range.
7 15:55:44 2602171514-0-7-n42665oc 10 PROTON ug2024 + + - + + + + Exp 4 Product || 1H Experiment
6 15:52:47 2602171514-0-6-t33197tl 11 C13CPD32 ug2024 - + - - - + + Exp_4_2_Y2 || COSY Exp_4_2_Y2 || 13C Experiment, 1H decoupled, 32 scans
6 15:45:38 2602171514-0-6-t33197tl 10 PROTON ug2024 + + - + + + +
5 15:42:46 2602171506-0-5-k34788la 11 C13CPD32 ug2024 - + - - - + + SuzukimiyauraLA || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602171506-0-5-k34788la/11/pdata/1/peaks No peaks found in the specified range.
5 15:35:12 2602171506-0-5-k34788la 10 PROTON ug2024 + + - + + + + SuzukimiyauraLA || 1H Experiment
4 15:32:19 2602171504-0-4-e83232ek 11 C13CPD32 ug2024 - + - - - + + ellishakoseexp4 || 13C Experiment, 1H decoupled, 32 scans
4 15:25:39 2602171504-0-4-e83232ek 10 PROTON ug2024 + + - + + + + ellishakoseexp4 || 1H Experiment
3 15:19:31 2602171504-0-3-m93350cd 11 COSYGPSW ug2024 - + - - - + + m93350cd || COSY
3 15:12:55 2602171504-0-3-m93350cd 10 PROTON ug2024 + + - + + + + m93350cd || 1H Experiment
2 15:10:00 2602171503-0-2-r87645as 11 C13CPD32 ug2024 - + - - - + + exp4suzukimiyaaura || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602171503-0-2-r87645as/11/pdata/1/peaks No peaks found in the specified range.
2 15:03:34 2602171503-0-2-r87645as 10 PROTON ug2024 + + - + + + + exp4suzukimiyaaura || 1H Experiment
1 14:50:58 2602171433-0-1-t33197tl 12 COSYGPSW ug2024 - + - - - + + Exp_4_Y2 || COSY
1 14:47:14 2602171433-0-1-t33197tl 11 C13CPD32 ug2024 - + - - - + + Exp_4_Y2 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602171433-0-1-t33197tl/11/pdata/1/peaks No peaks found in the specified range.
1 14:40:24 2602171433-0-1-t33197tl 10 PROTON ug2024 + + - + + + + Exp_4_Y2 || 1H Experiment
14 20:04:02 2602161615-0-14-q84930bb 15 F19 ug2023 - + - - - + + in_situ-trifluoroacetylation_Monday || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
14 18:56:37 2602161615-0-14-q84930bb 14 C13CPD ug2023 - + - - - + + in_situ-trifluoroacetylation_Monday || 13C Experiment, 1H decoupled, 128 scans
14 17:00:16 2602161615-0-14-q84930bb 13 HMBCLPND ug2023 - + - - - + + in_situ-trifluoroacetylation_Monday || Long range 1H-13C correlation
14 16:45:13 2602161615-0-14-q84930bb 12 HSQCEDETGP ug2023 - + - - - + + in_situ-trifluoroacetylation_Monday || 1-bond 1H-13C correlation with CH/CH3 up and CH2 down
14 16:39:06 2602161615-0-14-q84930bb 11 COSYGPSW ug2023 - + - - - + + in_situ-trifluoroacetylation_Monday || COSY
14 16:28:19 2602161615-0-14-q84930bb 10 PROTON ug2023 + + - + + + + in_situ-trifluoroacetylation_Monday || 1H Experiment
13 16:20:22 2602161540-0-13-v67557bm 10 PROTON teaching + + - + + + + andrew.ralph@student.manchester.ac.uk || 1H Experiment
12 16:12:48 2602161540-0-12-v67557bm 10 PROTON teaching + + - + + + + jack.hodge@student.manchester.ac.uk || 1H Experiment
11 16:06:42 2602161540-0-11-v67557bm 10 PROTON teaching + + - + + + + megan.glaser@student.manchester.ac.uk || 1H Experiment
10 15:59:46 2602161533-0-10-e46528zs 10 PROTON ug2025 + + - + + + + sunzeen-exp14 || 1H Experiment
9 15:44:15 2602161530-0-9-g94420dm 10 PROTON ug2025 + + - + + + + Scarlett Experiment 14 || 1H Experiment
8 15:37:49 2602161530-0-8-g94420dm 10 PROTON ug2025 + + - + + + + Darcey Experiment 14 || 1H Experiment
7 15:27:36 2602161526-0-7-f14505lh 10 PROTON ug2025 + + - + + + + Leo-exp14 nbh4 || 1H Experiment
6 14:35:41 2602161321-0-6-t19785ak 10 PROTON ug2023 + + - + + + + 120 degrees 4-ep+4-vp oil withb internal standard || 1H Experiment
5 14:27:14 20260216-1112-B300_2.044-5 15 PROTON y1-K/E + + - + + + + Ref Acteyl Acetone
4 14:21:04 20260216-1110-B300_2.044-4 15 PROTON y1-K/E + + - + + + + Ref 1-phenylbutane-1,3-dione
3 14:13:40 20260216-1043-B300_2.044-3 15 PROTON y1-K/E + + - + + + + Ref phenyl
5 14:07:25 20260216-1112-B300_2.044-5 14 PROTON y1-K/E + + - + + + + Ref Acteyl Acetone
2 14:00:00 20260216-1041-B300_2.044-2 15 PROTON y1-K/E + + - + + + + Ref Eth7yl acetoate
4 13:51:29 20260216-1110-B300_2.044-4 14 PROTON y1-K/E + + - + + + + Ref 1-phenylbutane-1,3-dione
1 13:44:31 20260216-1038-B300_2.044-1 15 PROTON y1-K/E + + - + + + + Ref acetylacetone in CDCl3
3 13:35:43 20260216-1043-B300_2.044-3 14 PROTON y1-K/E + + - + + + + Ref phenyl
5 13:27:07 20260216-1112-B300_2.044-5 13 PROTON y1-K/E + + - + + + + Ref Acteyl Acetone
2 13:17:54 20260216-1041-B300_2.044-2 14 PROTON y1-K/E + + - + + + + Ref Eth7yl acetoate
4 13:11:30 20260216-1110-B300_2.044-4 13 PROTON y1-K/E + + - + + + + Ref 1-phenylbutane-1,3-dione
1 13:03:03 20260216-1038-B300_2.044-1 14 PROTON y1-K/E + + - + + + + Ref acetylacetone in CDCl3
3 12:55:08 20260216-1043-B300_2.044-3 13 PROTON y1-K/E + + - + + + + Ref phenyl
5 12:47:27 20260216-1112-B300_2.044-5 12 PROTON y1-K/E + + - + + + + Ref Acteyl Acetone
2 12:38:07 20260216-1041-B300_2.044-2 13 PROTON y1-K/E + + - + + + + Ref Eth7yl acetoate
4 12:31:19 20260216-1110-B300_2.044-4 12 PROTON y1-K/E + + - + + + + Ref 1-phenylbutane-1,3-dione
1 12:24:19 20260216-1038-B300_2.044-1 13 PROTON y1-K/E + + - + + + + Ref acetylacetone in CDCl3
3 12:17:21 20260216-1043-B300_2.044-3 12 PROTON y1-K/E + + - + + + + Ref phenyl
5 12:09:43 20260216-1112-B300_2.044-5 11 PROTON y1-K/E + + - + + + + Ref Acteyl Acetone
2 12:01:00 20260216-1041-B300_2.044-2 12 PROTON y1-K/E + + - + + + + Ref Eth7yl acetoate
4 11:54:41 20260216-1110-B300_2.044-4 11 PROTON y1-K/E + + - + + + + Ref 1-phenylbutane-1,3-dione
1 11:46:46 20260216-1038-B300_2.044-1 12 PROTON y1-K/E + + - + + + + Ref acetylacetone in CDCl3
3 11:37:34 20260216-1043-B300_2.044-3 11 PROTON y1-K/E + + - + + + + Ref phenyl
5 11:30:50 20260216-1112-B300_2.044-5 10 PROTON y1-K/E + + - + + + + Ref Acteyl Acetone
2 11:21:33 20260216-1041-B300_2.044-2 11 PROTON y1-K/E + + - + + + + Ref Eth7yl acetoate
4 11:14:49 20260216-1110-B300_2.044-4 10 PROTON y1-K/E + + - + + + + Ref 1-phenylbutane-1,3-dione
1 11:08:00 20260216-1038-B300_2.044-1 11 PROTON y1-K/E + + - + + + + Ref acetylacetone in CDCl3
3 10:53:24 20260216-1043-B300_2.044-3 10 PROTON y1-K/E + + - + + + + Ref phenyl
2 10:46:47 20260216-1041-B300_2.044-2 10 PROTON y1-K/E + + - + + + + Ref Eth7yl acetoate
1 10:40:56 20260216-1038-B300_2.044-1 10 PROTON y1-K/E + + - + + + + Ref acetylacetone in CDCl3
15 19:35:06 2602121059-0-15-r36807jm 10 PROTON ug2023 x - - - - - - N-tert butyl amide || 1H Experiment SampleChanger Error: 1000 SampleTransportController: No Sample at requested Position.
11 18:23:47 2602131536-0-11-y42534zw 10 C13CPD ug2023 + + - + + + + G38S3 1 4N 16-21 || 13C Experiment, 1H decoupled, 128 scans
10 17:12:50 2602131536-0-10-y42534zw 10 C13CPD ug2023 + + - + + + + G38S3 1 product345 || 13C Experiment, 1H decoupled, 128 scans
9 16:00:56 2602131536-0-9-y42534zw 10 C13CPD ug2023 + + - + + + + G38 S4 w2 || 13C Experiment, 1H decoupled, 128 scans
29 10:34:35 2602131434-0-29-p12908lh 10 PROTON ug2023 + + - + + + + 2.12 cat. || 1H Experiment
24 10:27:36 2602131431-0-24-p12908lh 10 PROTON ug2023 + + - + + + + 2.13 EtOH:H2O=1:1 || 1H Experiment
23 10:19:35 2602131431-0-23-p12908lh 10 PROTON ug2023 + + - + + + + 2.13 EtOH:H2O=3:1 || 1H Experiment
22 10:10:42 2602131431-0-22-p12908lh 10 PROTON ug2023 + + - + + + + 2.12 EtOH:H2O=3:1 || 1H Experiment
12 10:08:55 2602131628-0-12-h38145ak 11 F19 ug2023 - + - - - + + allylic acylation || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
12 09:59:17 2602131628-0-12-h38145ak 10 PROTON ug2023 + + - + + + + allylic acylation || 1H Experiment
8 09:56:24 2602131532-0-8-c22796za 11 C13CPD32 ug2023 - + - - - + + Aqeuous layer of NHC (probably nothing) || 13C Experiment, 1H decoupled, 32 scans
8 09:49:15 2602131532-0-8-c22796za 10 PROTON ug2023 + + - + + + + Aqeuous layer of NHC (probably nothing) || 1H Experiment
5 09:37:14 2602131516-0-5-r99959zh 10 PROTON ug2023 + + - + + + + G3R1 FEE solvent || 1H Experiment
4 09:29:21 2602131516-0-4-r99959zh 10 PROTON ug2023 + + - + + + + G3R1 FEE Solid || 1H Experiment
7 09:25:39 2602131524-0-7-a59382yh 11 C13CPD32 ug2023 - + - - - + + Aniineextraction2 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131524-0-7-a59382yh/11/pdata/1/peaks No peaks found in the specified range.
7 09:18:12 2602131524-0-7-a59382yh 10 PROTON ug2023 + + - + + + + Aniineextraction2 || 1H Experiment
6 09:11:44 2602131517-0-6-q09060yz 10 PROTON ug2023 + + - + + + + yier 13.2 || 1H Experiment
3 09:09:23 2602131514-0-3-d54865hg 12 P31CPD ug2023 - + - - - + + electro pt 4 || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
3 09:05:52 2602131514-0-3-d54865hg 11 C13CPD32 ug2023 - + - - - + + electro pt 4 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131514-0-3-d54865hg/11/pdata/1/peaks No peaks found.
3 08:57:06 2602131514-0-3-d54865hg 10 PROTON ug2023 + + - + + + + electro pt 4 || 1H Experiment
60 08:54:35 2602131508-0-60-z34413sw 10 PROTON ug2023 + + - x - - - G14-AK-4 || 1H Experiment Lock failed after multiple attempts, lock: Command 'lock CDCl3' failed. Lock is OFF, Command 'lock CDCl3' failed. Lock is OFF
59 08:51:40 2602131502-0-59-d98689cd 11 C13CPD32 ug2023 - + - - - + + G32 Coupling || 13C Experiment, 1H decoupled, 32 scans
59 08:44:45 2602131502-0-59-d98689cd 10 PROTON ug2023 + + - + + + + G32 Coupling || 1H Experiment
49 08:41:51 2602131500-0-49-v45005oc 11 C13CPD32 ug2023 - + - - - + + CHOLESTANOL SM || 13C Experiment, 1H decoupled, 32 scans
49 08:34:53 2602131500-0-49-v45005oc 10 PROTON ug2023 + + - + + + + CHOLESTANOL SM || 1H Experiment
58 08:32:02 2602131501-0-58-c68704nm 11 C13CPD32 ug2023 - + - - - + + Dini Part2 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131501-0-58-c68704nm/11/pdata/1/peaks No peaks found in the specified range.
58 08:22:17 2602131501-0-58-c68704nm 10 PROTON ug2023 + + - + + + + Dini Part2 || 1H Experiment
47 08:14:43 2602131452-0-47-t19785ak 10 PROTON ug2023 + + - + + + + 4-ep 110 degrees 2 hours plus product || 1H Experiment
48 08:03:54 2602131452-0-48-t19785ak 10 PROTON ug2023 + + - + + + + A 110 de3grees 2 hpoura plus || 1H Experiment
35 08:01:01 2602131449-0-35-a59382yh 11 C13CPD32 ug2023 - + - - - + + Anilineextraction1 || 13C Experiment, 1H decoupled, 32 scans
35 07:52:33 2602131449-0-35-a59382yh 10 PROTON ug2023 + + - + + + + Anilineextraction1 || 1H Experiment
34 07:44:20 2602131448-0-34-b35901ws 10 PROTON ug2023 + + - + + + + 110 60 mins || 1H Experiment
33 07:38:20 2602131448-0-33-b35901ws 10 PROTON ug2023 + + - + + + + 100 60 mins || 1H Experiment
32 07:31:34 2602131443-0-32-q09060yz 10 PROTON ug2023 + + - + + + + lydia 13.2 pddppfcl2 || 1H Experiment
28 07:26:08 2602131437-0-28-c37210bx 11 C13CPD32 ug2023 - + - - - + + 18-crown-6 || 13C Experiment, 1H decoupled, 32 scans
28 07:18:32 2602131437-0-28-c37210bx 10 PROTON ug2023 + + - + + + + 18-crown-6 || 1H Experiment
27 07:14:47 2602131437-0-27-c37210bx 11 C13CPD32 ug2023 - + - - - + + LDA base || 13C Experiment, 1H decoupled, 32 scans
27 07:06:53 2602131437-0-27-c37210bx 10 PROTON ug2023 + + - + + + + LDA base || 1H Experiment
30 07:05:15 2602131433-0-30-s81742yz 12 F19 ug2023 - + - - - + + W2D2W1product || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
30 05:57:49 2602131433-0-30-s81742yz 11 C13CPD ug2023 - + - - - + + W2D2W1product || 13C Experiment, 1H decoupled, 128 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131433-0-30-s81742yz/11/pdata/1/peaks No peaks found in the specified range.
30 05:48:51 2602131433-0-30-s81742yz 10 PROTON ug2023 + + - + + + + W2D2W1product || 1H Experiment
18 05:42:04 2602131434-0-18-n98843hm 10 PROTON ug2023 + + - + + + + piperidine_110*_40m_13/02 || 1H Experiment
17 05:32:31 2602131434-0-17-n98843hm 10 PROTON ug2023 + + - + + + + piperidine_120*_2hr_13/02 || 1H Experiment
1 05:23:47 2602131434-0-1-n98843hm 10 PROTON ug2023 + + - + + + + piperidine_110*_1hr_13/02 || 1H Experiment
16 04:09:47 2602131347-0-16-mbdssmh7 11 C13CPD teaching + + - + + + + MJH_Y1_Ketal_ || 13C Experiment, 1H decoupled, 128 scans
46 04:06:01 2602131338-0-46-d54865hg 11 C13CPD32 ug2023 - + - - - + + prenol || 13C Experiment, 1H decoupled, 32 scans
46 03:59:21 2602131338-0-46-d54865hg 10 PROTON ug2023 + + - + + + + prenol || 1H Experiment
45 03:57:09 2602131338-0-45-d54865hg 12 P31CPD ug2023 - + - - - + + electro pt 3 || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
45 03:54:03 2602131338-0-45-d54865hg 11 C13CPD32 ug2023 - + - - - + + electro pt 3 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131338-0-45-d54865hg/11/pdata/1/peaks No peaks found.
45 03:48:08 2602131338-0-45-d54865hg 10 PROTON ug2023 + + - + + + + electro pt 3 || 1H Experiment
57 03:42:27 2602131336-0-57-m00673hs 10 PROTON ug2023 + + - + + + + Strong Proline || 1H Experiment
56 03:36:42 2602131336-0-56-m00673hs 10 PROTON ug2023 + + - + + + + Blank All || 1H Experiment
55 03:30:31 2602131336-0-55-m00673hs 10 PROTON ug2023 + + - + + + + Blank Glucose || 1H Experiment
54 03:24:46 2602131336-0-54-m00673hs 10 PROTON ug2023 + + - + + + + Blank HMF || 1H Experiment
53 03:18:31 2602131336-0-53-m00673hs 10 PROTON ug2023 + + - + + + + Blank Proline || 1H Experiment
44 03:10:00 2602131333-0-44-m20809op 10 PROTON ug2023 + + - + + + + 23 solid || 1H Experiment
43 03:03:06 2602131333-0-43-m20809op 10 PROTON ug2023 + + - + + + + 23 liquid || 1H Experiment
50 03:00:13 2602131336-0-50-j80847ja 11 C13CPD32 ug2023 - + - - - + + jood- limonene product (no column) || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131336-0-50-j80847ja/11/pdata/1/peaks No peaks found in the specified range.
50 02:52:39 2602131336-0-50-j80847ja 10 PROTON ug2023 + + - + + + + jood- limonene product (no column) || 1H Experiment
51 02:49:45 2602131336-0-51-j80847ja 11 C13CPD32 ug2023 - + - - - + + ben- limonene product (no column) || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131336-0-51-j80847ja/11/pdata/1/peaks No peaks found in the specified range.
51 02:42:43 2602131336-0-51-j80847ja 10 PROTON ug2023 + + - + + + + ben- limonene product (no column) || 1H Experiment
52 02:39:51 2602131336-0-52-j80847ja 11 C13CPD32 ug2023 - + - - - + + lee- gamma terpinene (no column || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131336-0-52-j80847ja/11/pdata/1/peaks No peaks found in the specified range.
52 02:32:39 2602131336-0-52-j80847ja 10 PROTON ug2023 + + - + + + + lee- gamma terpinene (no column || 1H Experiment
42 02:29:48 2602131321-0-42-c22796za 11 C13CPD32 ug2023 - + - - - + + NHC1 REDWINESAMPLE in Et2O || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131321-0-42-c22796za/11/pdata/1/peaks No peaks found in the specified range.
42 02:22:59 2602131321-0-42-c22796za 10 PROTON ug2023 + + - + + + + NHC1 REDWINESAMPLE in Et2O || 1H Experiment
39 01:11:44 2602131306-0-39-z73813ns 10 C13CPD ug2023 + + - + + + + NS Crude Carbodiimide D 13C || 13C Experiment, 1H decoupled, 128 scans
38 00:00:21 2602131306-0-38-z73813ns 10 C13CPD ug2023 + + - + + + + NS Urea D 13C || 13C Experiment, 1H decoupled, 128 scans
37 23:51:11 2602131306-0-37-z73813ns 10 PROTON ug2023 + + - + + + + NS Urea D R2 runoff 1H || 1H Experiment
41 23:42:42 2602131308-0-41-z34413sw 10 PROTON ug2023 + + - + + + + G14-trifluro || 1H Experiment
40 23:39:48 2602131305-0-40-g10446rm 11 C13CPD32 ug2023 - + - - - + + RM_Green_Tar || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131305-0-40-g10446rm/11/pdata/1/peaks No peaks found in the specified range.
40 23:33:26 2602131305-0-40-g10446rm 10 PROTON ug2023 + + - + + + + RM_Green_Tar || 1H Experiment
36 23:29:45 2602131303-0-36-g10446rm 11 C13CPD32 ug2023 - + - - - + + RM_L15_#2 || 13C Experiment, 1H decoupled, 32 scans
36 23:21:40 2602131303-0-36-g10446rm 10 PROTON ug2023 + + - + + + + RM_L15_#2 || 1H Experiment
13 23:19:59 2602131110-0-13-s81742yz 12 F19 ug2023 - + - - - + + W2D226biCF3aniline || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
13 22:07:14 2602131110-0-13-s81742yz 11 C13CPD ug2023 + + - + + + + W2D226biCF3aniline || 13C Experiment, 1H decoupled, 128 scans
2 20:04:11 2602131023-0-2-c68402hw 14 HMBCLPND ug2023 - + - - - + + Urea B Full Data || Long range 1H-13C correlation
2 19:48:22 2602131023-0-2-c68402hw 13 HSQCEDETGP ug2023 - + - - - + + Urea B Full Data || 1-bond 1H-13C correlation with CH/CH3 up and CH2 down
2 19:42:14 2602131023-0-2-c68402hw 12 COSYGPSW ug2023 - + - - - + + Urea B Full Data || COSY
2 18:34:43 2602131023-0-2-c68402hw 11 C13CPD ug2023 - + - - - + + Urea B Full Data || 13C Experiment, 1H decoupled, 128 scans
2 18:29:20 2602131023-0-2-c68402hw 10 PROTON ug2023 + + - + + + + Urea B Full Data || 1H Experiment
21 17:17:55 2602121122-0-21-y42534zw 10 C13CPD ug2023 + + - + + + + G38 S3 || 13C Experiment, 1H decoupled, 128 scans
20 16:06:14 2602121122-0-20-y42534zw 10 C13CPD ug2023 + + - + + + + G38 S4 || 13C Experiment, 1H decoupled, 128 scans
26 16:03:22 2602131437-0-26-c37210bx 11 C13CPD32 ug2023 - + - - - + + CRUDE Na || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131437-0-26-c37210bx/11/pdata/1/peaks No peaks found in the specified range.
26 15:57:08 2602131437-0-26-c37210bx 10 PROTON ug2023 + + - + + + + CRUDE Na || 1H Experiment
25 15:54:16 2602131437-0-25-c37210bx 11 C13CPD32 ug2023 - + - - - + + crude LDA || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131437-0-25-c37210bx/11/pdata/1/peaks No peaks found in the specified range.
25 15:46:53 2602131437-0-25-c37210bx 10 PROTON ug2023 + + - + + + + crude LDA || 1H Experiment
19 15:43:51 2602131258-0-19-j43382nb 11 C13CPD32 ug2023 - + - - - + + Fluoxetine hydrochloride || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131258-0-19-j43382nb/11/pdata/1/peaks No peaks found in the specified range.
19 15:36:09 2602131258-0-19-j43382nb 10 PROTON ug2023 + + - + + + + Fluoxetine hydrochloride || 1H Experiment
16 15:29:00 2602131347-0-16-mbdssmh7 10 PROTON teaching + + - + + + + MJH_Y1_Ketal_ || 1H Experiment
14 15:21:50 2602131112-0-14-t16779zc 10 PROTON ug2023 + + - + + + + tffa rhodamine 110 || 1H Experiment
12 15:18:58 2602131258-0-12-j43382nb 11 C13CPD32 ug2023 - + - - - + + Lidocaine || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131258-0-12-j43382nb/11/pdata/1/peaks No peaks found in the specified range.
12 15:12:44 2602131258-0-12-j43382nb 10 PROTON ug2023 + + - + + + + Lidocaine || 1H Experiment
11 15:09:52 2602131244-0-11-r27389ac 11 C13CPD32 ug2023 - + - - - + + Napthalene-methanol || 13C Experiment, 1H decoupled, 32 scans
11 15:03:40 2602131244-0-11-r27389ac 10 PROTON ug2023 + + - + + + + Napthalene-methanol || 1H Experiment
10 15:00:42 2602131242-0-10-j77257is 11 C13CPD32 ug2023 - + - - - + + Holly fraction 1 || 13C Experiment, 1H decoupled, 32 scans
10 14:51:53 2602131242-0-10-j77257is 10 PROTON ug2023 + + - + + + + Holly fraction 1 || 1H Experiment
9 14:48:54 2602131242-0-9-j77257is 11 C13CPD32 ug2023 - + - - - + + Isa fraction 3 || 13C Experiment, 1H decoupled, 32 scans
9 14:41:20 2602131242-0-9-j77257is 10 PROTON ug2023 + + - + + + + Isa fraction 3 || 1H Experiment
8 14:38:22 2602131242-0-8-j77257is 11 C13CPD32 ug2023 - + - - - + + Isa fraction 2 || 13C Experiment, 1H decoupled, 32 scans
8 14:30:25 2602131242-0-8-j77257is 10 PROTON ug2023 + + - + + + + Isa fraction 2 || 1H Experiment
7 14:27:29 2602131238-0-7-j09499ww 11 C13CPD32 ug2023 - + - - - + + L15 WS #2 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131238-0-7-j09499ww/11/pdata/1/peaks No peaks found in the specified range.
7 14:20:46 2602131238-0-7-j09499ww 10 PROTON ug2023 + + - + + + + L15 WS #2 || 1H Experiment
6 14:15:32 2602131216-0-6-k03256gd 10 PROTON ug2023 + + - + + + + C filtrate || 1H Experiment
5 14:10:16 2602131216-0-5-k03256gd 10 PROTON ug2023 + + - + + + + Urea C (2) || 1H Experiment
4 14:07:21 2602131210-0-4-j09499ww 11 C13CPD32 ug2023 - + - - - + + L15 WS #1 || 13C Experiment, 1H decoupled, 32 scans
4 14:00:22 2602131210-0-4-j09499ww 10 PROTON ug2023 + + - + + + + L15 WS #1 || 1H Experiment
3 13:57:02 2602131210-0-3-j09499ww 11 C13CPD32 ug2023 - + - - - + + L15 LH #1 || 13C Experiment, 1H decoupled, 32 scans
3 13:50:11 2602131210-0-3-j09499ww 10 PROTON ug2023 + + - + + + + L15 LH #1 || 1H Experiment
1 13:48:29 2602131205-0-1-z73813ns 10 PROTON ug2023 x - - - - - - NS Urea D R2 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
35 13:48:26 2602131256-0-35-j42917hk 10 PROTON ug2023 x - - - - - - Group 23 HK || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
34 13:48:11 2602131256-0-34-j42917hk 10 PROTON ug2023 x - - - - - - Group 23 NO || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Inconsistent Inputs detected by Controller, please check light barriers. SMCB input word: 0x00021B43
33 13:45:13 2602131258-0-33-j43382nb 11 C13CPD32 ug2023 - + - - - + + Procaine hydrochloride || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131258-0-33-j43382nb/11/pdata/1/peaks No peaks found in the specified range.
33 13:36:42 2602131258-0-33-j43382nb 10 PROTON ug2023 + + - + + + + Procaine hydrochloride || 1H Experiment
32 13:33:50 2602131258-0-32-j43382nb 11 C13CPD32 ug2023 - + - - - + + Fmoc Cl || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131258-0-32-j43382nb/11/pdata/1/peaks No peaks found in the specified range.
32 13:27:34 2602131258-0-32-j43382nb 10 PROTON ug2023 + + - + + + + Fmoc Cl || 1H Experiment
31 13:20:50 2602131201-0-31-t69807al 10 PROTON ug2023 + + - + + + + crude urea || 1H Experiment
30 13:15:37 2602131154-0-30-d24415td 10 PROTON ug2023 + + - + + + + TD thread 1 || 1H Experiment
29 13:10:31 2602131152-0-29-k03256gd 10 PROTON ug2023 + + - + + + + Separation B || 1H Experiment
28 13:05:02 2602131151-0-28-n77009rc 10 PROTON ug2023 + + - + + + + Wildflower 3 || 1H Experiment
27 12:59:24 2602131151-0-27-n77009rc 10 PROTON ug2023 + + - + + + + Blank All || 1H Experiment
26 12:53:46 2602131151-0-26-n77009rc 10 PROTON ug2023 + + - + + + + Blank Glucose || 1H Experiment
25 12:47:33 2602131151-0-25-n77009rc 10 PROTON ug2023 + + - + + + + Blank HMF || 1H Experiment
24 12:41:51 2602131151-0-24-n77009rc 10 PROTON ug2023 + + - + + + + Blank Proline || 1H Experiment
23 12:38:56 2602131142-0-23-j77257is 11 C13CPD32 ug2023 - + - - - + + Isa fraction 1 || 13C Experiment, 1H decoupled, 32 scans
23 12:30:38 2602131142-0-23-j77257is 10 PROTON ug2023 + + - + + + + Isa fraction 1 || 1H Experiment
22 12:21:57 2602131140-0-22-r99959zh 10 PROTON ug2023 + + - + + + + G3R1 FEE || 1H Experiment
18 12:19:05 2602131137-0-18-a59382yh 11 C13CPD32 ug2023 - + - - - + + YH_4Aminobenzonitrile || 13C Experiment, 1H decoupled, 32 scans
18 12:10:04 2602131137-0-18-a59382yh 10 PROTON ug2023 + + - + + + + YH_4Aminobenzonitrile || 1H Experiment
17 12:04:26 2602131124-0-17-k03256gd 10 PROTON ug2023 + + - + + + + Amine C || 1H Experiment
16 12:01:28 2602131117-0-16-j82035sh 11 C13CPD32 ug2023 - + - - - + + StanCrudeProdNoSolvent || 13C Experiment, 1H decoupled, 32 scans
16 11:54:42 2602131117-0-16-j82035sh 10 PROTON ug2023 + + - + + + + StanCrudeProdNoSolvent || 1H Experiment
13 11:48:24 2602131110-0-13-s81742yz 10 PROTON ug2023 + + - + + + + W2D226biCF3aniline || 1H Experiment
12 11:45:53 2602131109-0-12-z34413sw 10 PROTON ug2023 + + - x - - - G14-AK-3 || 1H Experiment Lock failed after multiple attempts, lock: Command 'lock CDCl3' failed. Lock is OFF, Command 'lock CDCl3' failed. Lock is OFF
11 11:42:56 2602131104-0-11-d94069rz 11 C13CPD32 ug2023 - + - - - + + shoujun coiii dmso || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131104-0-11-d94069rz/11/pdata/1/peaks No peaks found in the specified range.
11 11:37:11 2602131104-0-11-d94069rz 10 PROTON ug2023 + + - + + + + shoujun coiii dmso || 1H Experiment
10 11:34:18 2602131103-0-10-j43382nb 11 C13CPD32 ug2023 - + - - - + + PMB protected quinine || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131103-0-10-j43382nb/11/pdata/1/peaks No peaks found in the specified range.
10 11:28:29 2602131103-0-10-j43382nb 10 PROTON ug2023 + + - + + + + PMB protected quinine || 1H Experiment
9 11:25:37 2602131103-0-9-j43382nb 11 C13CPD32 ug2023 - + - - - + + Quinine || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131103-0-9-j43382nb/11/pdata/1/peaks No peaks found in the specified range.
9 11:19:50 2602131103-0-9-j43382nb 10 PROTON ug2023 + + - + + + + Quinine || 1H Experiment
8 11:10:57 2602131033-0-8-z82227gm 10 PROTON ug2023 + + - + + + + Product of reaction || 1H Experiment
7 11:02:25 2602131033-0-7-z82227gm 10 PROTON ug2023 + + - + + + + Rhodamine 6g starting material || 1H Experiment
6 10:53:51 2602131032-0-6-z34413sw 10 PROTON ug2023 + + - + + + + CDCl3 || 1H Experiment
5 10:45:50 2602131032-0-5-z34413sw 10 PROTON ug2023 + + - + + + + G14-OMe-3 || 1H Experiment
4 10:42:52 2602131024-0-4-d94069rz 11 C13CPD32 ug2023 - + - - - + + ruogu amide || 13C Experiment, 1H decoupled, 32 scans
4 10:34:21 2602131024-0-4-d94069rz 10 PROTON ug2023 + + - + + + + ruogu amide || 1H Experiment
3 10:31:29 2602131024-0-3-d94069rz 11 C13CPD32 ug2023 - + - - - + + shoujun coiii || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602131024-0-3-d94069rz/11/pdata/1/peaks No peaks found in the specified range.
3 10:25:28 2602131024-0-3-d94069rz 10 PROTON ug2023 + + - + + + + shoujun coiii || 1H Experiment
1 10:21:51 2602131013-0-1-j82035sh 11 C13CPD32 ug2023 - + - - - + + DBTRef || 13C Experiment, 1H decoupled, 32 scans
1 10:13:26 2602131013-0-1-j82035sh 10 PROTON ug2023 + + - + + + + DBTRef || 1H Experiment
35 07:48:15 2602121548-0-35-j80847ja 11 C13CPD32 ug2023 - + - - - + + limonene ben bottom layer || 13C Experiment, 1H decoupled, 32 scans
35 07:39:44 2602121548-0-35-j80847ja 10 PROTON ug2023 + + - + + + + limonene ben bottom layer || 1H Experiment
34 07:36:46 2602121548-0-34-j80847ja 11 C13CPD32 ug2023 - + - - - + + limonene Ben top layer || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602121548-0-34-j80847ja/11/pdata/1/peaks No peaks found in the specified range.
34 07:28:42 2602121548-0-34-j80847ja 10 PROTON ug2023 + + - + + + + limonene Ben top layer || 1H Experiment
33 07:25:45 2602121545-0-33-r98087nv 11 C13CPD32 ug2023 - + - - - + + Protection Product P. HCL || 13C Experiment, 1H decoupled, 32 scans
33 07:19:27 2602121545-0-33-r98087nv 10 PROTON ug2023 + + - + + + + Protection Product P. HCL || 1H Experiment
32 07:14:07 2602121540-0-32-d24415td 10 PROTON ug2023 + + - + + + + MS Thread 1 || 1H Experiment
31 07:11:10 2602121538-0-31-j82035sh 11 C13CPD32 ug2023 - + - - - + + StanCrudeDBToxideDCM || 13C Experiment, 1H decoupled, 32 scans
31 07:01:16 2602121538-0-31-j82035sh 10 PROTON ug2023 + + - + + + + StanCrudeDBToxideDCM || 1H Experiment
30 06:54:34 2602121532-0-30-r99959zh 10 PROTON ug2023 + + - + + + + G3 FEE 2.0 || 1H Experiment
29 06:45:33 2602121532-0-29-r99959zh 10 PROTON ug2023 + + - + + + + G3 FEE 1.0 || 1H Experiment
27 06:39:18 2602121510-0-27-z34413sw 10 PROTON ug2023 + + - + + + + G14-OMe-2 || 1H Experiment
26 05:31:10 2602121457-0-26-z91447bd 11 C13CPD ug2023 - + - - - + + Purified Benzoyl 4-MU Ester || 13C Experiment, 1H decoupled, 128 scans
26 05:25:23 2602121457-0-26-z91447bd 10 PROTON ug2023 + + - + + + + Purified Benzoyl 4-MU Ester || 1H Experiment
25 05:23:17 2602121433-0-25-g14620tl 12 P31 ug2023 - + - - - + + PSI reagent hydrolysis || 31P Experiment, No Decoupling, 32 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0
25 05:21:11 2602121433-0-25-g14620tl 11 P31CPD ug2023 - + - - - + + PSI reagent hydrolysis || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0
25 05:14:25 2602121433-0-25-g14620tl 10 PROTON ug2023 + + - + + + + PSI reagent hydrolysis || 1H Experiment
24 05:04:13 2602121417-0-24-t19785ak 10 PROTON ug2023 + + - + + + + 4-ep+4-vp after 2 hour oil used 12/02/26 || 1H Experiment
23 04:54:24 2602121417-0-23-t19785ak 10 PROTON ug2023 + + - + + + + 4-Ep pure 12/02/26 || 1H Experiment
22 04:41:58 2602121417-0-22-t19785ak 10 PROTON ug2023 + + - + + + + 4-vp pure only 12/02/26 || 1H Experiment
18 04:34:30 2602121419-0-18-a98524wr 10 PROTON ug2023 + + - + + + + King-Jerry Thursday 12th Feb, Knoevenagel- Michael addition with hexanal and neutral alumina final product || 1H Experiment
17 04:26:01 2602121419-0-17-a98524wr 10 PROTON ug2023 + + - + + + + King-Jerry, Thursday 12th Feb, Knoevenagel- Michael addition with hexanal and neutral alumina 40 mins in || 1H Experiment
16 04:18:53 2602121419-0-16-a98524wr 10 PROTON ug2023 + + - + + + + King-Jerry, Thursday 12th Feb, Knoevenagel-Michael addition with hexanal and neutral alumina 30 mins in || 1H Experiment
14 04:11:17 2602121419-0-14-a98524wr 10 PROTON ug2023 + + - + + + + King-Jerry, Thursday 12th Feb, Knoevenagel- Michael addition with hexanal and neutral alumina 20 mins in || 1H Experiment
12 04:03:42 2602121419-0-12-a98524wr 10 PROTON ug2023 + + - + + + + King-Jerry, Thursday 12th Feb, Knoevenagel Adduct from hexanal || 1H Experiment
9 03:58:36 2602121353-0-9-c68402hw 10 PROTON ug2023 + + - + + + + unknown in column waste || 1H Experiment
8 03:55:36 2602121353-0-8-c68402hw 11 C13CPD32 ug2023 - + - - - + + carbodiimide B after column || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602121353-0-8-c68402hw/11/pdata/1/peaks No peaks found in the specified range.
8 03:49:37 2602121353-0-8-c68402hw 10 PROTON ug2023 + + - + + + + carbodiimide B after column || 1H Experiment
11 03:41:35 2602121353-0-11-q09060yz 10 PROTON ug2023 + + - + + + + lydia B pddppfcl2 || 1H Experiment
10 03:35:18 2602121353-0-10-q09060yz 10 PROTON ug2023 + + - + + + + yier A pdoac2 || 1H Experiment
7 03:32:25 2602121335-0-7-j80847ja 11 C13CPD32 ug2023 - + - - - + + limonene W1 jood product || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602121335-0-7-j80847ja/11/pdata/1/peaks No peaks found in the specified range.
7 03:23:58 2602121335-0-7-j80847ja 10 PROTON ug2023 + + - + + + + limonene W1 jood product || 1H Experiment
5 02:15:54 2602121322-0-5-z73813ns 11 C13CPD ug2023 - + - - - + + NS Carbodiimine D Pure || 13C Experiment, 1H decoupled, 128 scans
5 02:08:47 2602121322-0-5-z73813ns 10 PROTON ug2023 + + - + + + + NS Carbodiimine D Pure || 1H Experiment
6 02:06:41 2602121323-0-6-g14620tl 12 P31 ug2023 - + - - - + + PSI REAGENT CD3OD || 31P Experiment, No Decoupling, 32 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'MeOD' SR is set to 0.0
6 02:04:33 2602121323-0-6-g14620tl 11 P31CPD ug2023 - + - - - + + PSI REAGENT CD3OD || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'MeOD' SR is set to 0.0
6 01:58:41 2602121323-0-6-g14620tl 10 PROTON ug2023 + + - + + + + PSI REAGENT CD3OD || 1H Experiment
4 01:55:44 2602121321-0-4-a98524wr 11 C13CPD32 ug2023 - + - - - + + Harry Week 2 Thursday isobutyraldehyde 1:1 || 13C Experiment, 1H decoupled, 32 scans
4 01:49:26 2602121321-0-4-a98524wr 10 PROTON ug2023 + + - + + + + Harry Week 2 Thursday isobutyraldehyde 1:1 || 1H Experiment
2 01:46:28 2602121319-0-2-a98524wr 11 C13CPD32 ug2023 - + - - - + + Will Week 2 Thursday Reaction 2 butyraldehyde || 13C Experiment, 1H decoupled, 32 scans
2 01:39:44 2602121319-0-2-a98524wr 10 PROTON ug2023 + + - + + + + Will Week 2 Thursday Reaction 2 butyraldehyde || 1H Experiment
1 01:34:20 2602121319-0-1-n77009rc 10 PROTON ug2023 + + - + + + + Blank all || 1H Experiment
60 01:28:08 2602121308-0-60-n77009rc 10 PROTON ug2023 + + - + + + + blank hmf || 1H Experiment
59 01:21:55 2602121308-0-59-n77009rc 10 PROTON ug2023 + + - + + + + blank proline || 1H Experiment
58 01:15:44 2602121308-0-58-n77009rc 10 PROTON ug2023 + + - + + + + blank glucose || 1H Experiment
57 01:10:06 2602121308-0-57-n77009rc 10 PROTON ug2023 + + - + + + + wildflower hmf || 1H Experiment
56 01:04:27 2602121304-0-56-m00673hs 10 PROTON ug2023 + + - + + + + Wildflower Glucose || 1H Experiment
55 00:59:18 2602121304-0-55-m00673hs 10 PROTON ug2023 + + - + + + + Wildflower Proline || 1H Experiment
54 00:53:15 2602121304-0-54-m00673hs 10 PROTON ug2023 + + - + + + + Manuka3 Glucose || 1H Experiment
52 00:47:39 2602121304-0-52-m00673hs 10 PROTON ug2023 + + - + + + + Manuka3 HMF || 1H Experiment
51 00:42:29 2602121304-0-51-m00673hs 10 PROTON ug2023 + + - + + + + Manuka3 Proline || 1H Experiment
50 00:34:44 2602121259-0-50-j85765wh 10 PROTON ug2023 + + - + + + + 100morpholine || 1H Experiment
48 00:27:33 2602121252-0-48-k03256gd 10 PROTON ug2023 + + - + + + + Purified carbodiimide C || 1H Experiment
49 00:20:47 2602121257-0-49-p08684se 10 PROTON ug2023 + + - + + + + Sam Ellis L15 - 30 minutes reaction aliquot (maybe too much cdcl3) || 1H Experiment
47 00:17:51 2602121246-0-47-n11051eh 11 C13CPD32 ug2023 - + - - - + + Paraform prod || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602121246-0-47-n11051eh/11/pdata/1/peaks No peaks found in the specified range.
47 00:11:40 2602121246-0-47-n11051eh 10 PROTON ug2023 + + - + + + + Paraform prod || 1H Experiment
46 00:03:24 2602121244-0-46-n98843hm 10 PROTON ug2023 + + - + + + + Piperidine_1hr_100*_12/02 || 1H Experiment
45 23:59:40 2602121243-0-45-q84930bb 12 C13CPD32 ug2023 - + - - - + + TFAA Only || 13C Experiment, 1H decoupled, 32 scans
45 23:57:45 2602121243-0-45-q84930bb 11 F19 ug2023 - + - - - + + TFAA Only || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
45 23:50:41 2602121243-0-45-q84930bb 10 PROTON ug2023 + + - + + + + TFAA Only || 1H Experiment
44 22:43:15 2602121239-0-44-d96985hs 11 C13CPD ug2023 - + - - - + + HSWeek2thurs 1:1 nitro || 13C Experiment, 1H decoupled, 128 scans
44 22:36:11 2602121239-0-44-d96985hs 10 PROTON ug2023 + + - + + + + HSWeek2thurs 1:1 nitro || 1H Experiment
43 21:28:42 2602121235-0-43-a28784zr 11 C13CPD ug2023 - + - - - + + 233tri || 13C Experiment, 1H decoupled, 128 scans
43 21:22:28 2602121235-0-43-a28784zr 10 PROTON ug2023 + + - + + + + 233tri || 1H Experiment
42 20:13:58 2602121235-0-42-a28784zr 11 C13CPD ug2023 - + - - - + + 1Fluoro || 13C Experiment, 1H decoupled, 128 scans
42 20:06:49 2602121235-0-42-a28784zr 10 PROTON ug2023 + + - + + + + 1Fluoro || 1H Experiment
41 20:01:16 2602121234-0-41-d98689cd 10 P31CPD ug2023 + + - + + + + CD Catalyst Phosphorus NMR || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0
40 19:58:20 2602121214-0-40-d54865hg 12 P31 ug2023 - + - - - + + HG - electro pt2 || 31P Experiment, No Decoupling, 32 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
40 19:51:32 2602121214-0-40-d54865hg 11 C13CPD32 ug2023 + + - + + + + HG - electro pt2 || 13C Experiment, 1H decoupled, 32 scans
19 19:45:06 2602121120-0-19-m57057jd 13 COSYGPSW ug2023 - + - - - + + G11 JD 4b CF3 || COSY
19 19:43:24 2602121120-0-19-m57057jd 12 F19 ug2023 - + - - - + + G11 JD 4b CF3 || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
19 18:30:16 2602121120-0-19-m57057jd 11 C13CPD ug2023 + + - + + + + G11 JD 4b CF3 || 13C Experiment, 1H decoupled, 128 scans
13 18:28:35 2602121056-0-13-t29189mm 12 F19 ug2023 - + - - - + + alcohol G || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
13 17:16:52 2602121056-0-13-t29189mm 11 C13CPD ug2023 + + - + + + + alcohol G || 13C Experiment, 1H decoupled, 128 scans
3 17:13:56 2602121012-0-3-r36807jm 13 C13CPD32 ug2023 - + - - - + + n-tert-butyl amide || 13C Experiment, 1H decoupled, 32 scans
3 16:01:31 2602121012-0-3-r36807jm 12 C13CPD ug2023 + + - + + + + n-tert-butyl amide || 13C Experiment, 1H decoupled, 128 scans
40 15:55:45 2602121214-0-40-d54865hg 10 PROTON ug2023 + + - + + + + HG - electro pt2 || 1H Experiment
39 15:50:14 2602121212-0-39-k21450ms 10 C13CPD32 ug2023 + + - + + + + MS-thread3 C13 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602121212-0-39-k21450ms/10/pdata/1/peaks No peaks found in the specified range.
38 15:44:49 2602121212-0-38-k21450ms 10 C13CPD32 ug2023 + + - + + + + RN-thread3 C13 || 13C Experiment, 1H decoupled, 32 scans
37 15:42:04 2602121214-0-37-j77257is 11 PROTON ug2023 - + - - - + + Yuting product || 1H Experiment
37 15:35:47 2602121214-0-37-j77257is 10 C13CPD32 ug2023 + + - + + + + Yuting product || 13C Experiment, 1H decoupled, 32 scans
36 15:32:49 2602121220-0-36-a98524wr 11 C13CPD32 ug2023 - + - - - + + Will Week 2 Thursday Reaction 1 Butyraldehyde 1:1.1 || 13C Experiment, 1H decoupled, 32 scans
36 15:26:38 2602121220-0-36-a98524wr 10 PROTON ug2023 + + - + + + + Will Week 2 Thursday Reaction 1 Butyraldehyde 1:1.1 || 1H Experiment
35 15:24:08 2602121214-0-35-j77257is 11 PROTON ug2023 - + - - - + + 3-methoxy carbon || 1H Experiment
35 15:17:44 2602121214-0-35-j77257is 10 C13CPD32 ug2023 + + - + + + + 3-methoxy carbon || 13C Experiment, 1H decoupled, 32 scans
34 15:10:30 2602121214-0-34-j77257is 10 C13CPD32 ug2023 + + - + + + + Holly product week 1 || 13C Experiment, 1H decoupled, 32 scans
33 15:04:06 2602121214-0-33-j77257is 10 C13CPD32 ug2023 + + - + + + + Isa product week1 || 13C Experiment, 1H decoupled, 32 scans
32 15:02:25 2602121149-0-32-q84930bb 12 F19 ug2023 - + - - - + + Alcohol H 12_02 || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
32 14:58:46 2602121149-0-32-q84930bb 11 C13CPD32 ug2023 - + - - - + + Alcohol H 12_02 || 13C Experiment, 1H decoupled, 32 scans
32 14:52:41 2602121149-0-32-q84930bb 10 PROTON ug2023 + + - + + + + Alcohol H 12_02 || 1H Experiment
31 14:45:07 2602121158-0-31-m20809op 10 PROTON ug2023 + + - + + + + edward product || 1H Experiment
30 14:36:42 2602121158-0-30-m20809op 10 PROTON ug2023 + + - + + + + hana product || 1H Experiment
53 14:34:04 20260212-1209-B300_2.044-53 19 PROTON h91753cp - + - - - + + Ref 19F-monitor_test
53 14:25:01 20260212-1209-B300_2.044-53 18 F19CPD h91753cp + + - + + + + Ref 19F-monitor_test sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
53 14:11:31 20260212-1209-B300_2.044-53 17 PROTON h91753cp + + - + + + + Ref 19F-monitor_test
29 14:02:43 2602121158-0-29-m20809op 10 PROTON ug2023 + + - + + + + olivia product || 1H Experiment
53 13:55:00 20260212-1209-B300_2.044-53 16 F19CPD h91753cp + + - + + + + Ref 19F-monitor_test sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
28 13:48:14 2602121129-0-28-n77009rc 10 PROTON ug2023 + + - + + + + Manuka 3 || 1H Experiment
53 13:37:55 20260212-1209-B300_2.044-53 15 PROTON h91753cp + + - + + + + Ref 19F-monitor_test
27 13:31:03 2602121129-0-27-n77009rc 10 PROTON ug2023 + + - + + + + Manuka 2 || 1H Experiment
53 13:25:00 20260212-1209-B300_2.044-53 14 F19CPD h91753cp + + - + + + + Ref 19F-monitor_test sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
26 13:17:53 2602121129-0-26-n77009rc 10 PROTON ug2023 + + - + + + + Manuka 1 || 1H Experiment
8 13:08:00 2602121225-0-8-t69807al 10 PROTON ug2023 + + - + + + + purified carbodiimide A || 1H Experiment
53 13:05:22 20260212-1209-B300_2.044-53 13 PROTON h91753cp - + - - - + + Ref 19F-monitor_test
53 12:55:00 20260212-1209-B300_2.044-53 12 F19CPD h91753cp + + - + + + + Ref 19F-monitor_test sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
25 12:45:01 2602121231-0-25-t69807al 10 PROTON ug2023 + + - + + + + crude carbodiimide A || 1H Experiment
24 12:39:28 2602121123-0-24-m00673hs 10 PROTON ug2023 + + - + + + + Wildflower2 || 1H Experiment
23 12:33:57 2602121123-0-23-m00673hs 10 PROTON ug2023 + + - + + + + Wildflower1 || 1H Experiment
22 12:26:48 2602121123-0-22-m00673hs 10 PROTON ug2023 + + - + + + + Blank || 1H Experiment
24 12:26:03 2602121123-0-24-m00673hs 10 PROTON ug2023 x - - - - - - Wildflower2 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
23 12:26:00 2602121123-0-23-m00673hs 10 PROTON ug2023 x - - - - - - Wildflower1 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
22 12:25:45 2602121123-0-22-m00673hs 10 PROTON ug2023 x - - - - - - Blank || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Inconsistent Inputs detected by Controller, please check light barriers. SMCB input word: 0x00041B43
53 12:23:07 20260212-1209-B300_2.044-53 11 PROTON h91753cp - + - - - + + Ref 19F-monitor_test
53 12:14:28 20260212-1209-B300_2.044-53 10 F19CPD h91753cp + + - + + + + Ref 19F-monitor_test log_err:
In experiment: 1D_acquisition_data 3 1 /opt/topspin4.5.0/prog/curdir/nmrsu/topshimData
(Parameter Set = '')

'tr' not possible in 2D acquisition, sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
19 12:07:46 2602121120-0-19-m57057jd 10 PROTON ug2023 + + - + + + + G11 JD 4b CF3 || 1H Experiment
18 12:01:33 2602121117-0-18-z34413sw 10 PROTON ug2023 + + - + + + + G14-OMe-2 || 1H Experiment
17 11:54:53 2602121115-0-17-s05774bb 10 PROTON ug2023 + + - + + + + BB G11 R=Cl || 1H Experiment
16 11:48:13 2602121106-0-16-d37549ac 10 PROTON ug2023 + + - + + + + product with cdcl3 || 1H Experiment
14 11:45:18 2602121057-0-14-r27389ac 11 C13CPD32 ug2023 - + - - - + + NC W2 crude || 13C Experiment, 1H decoupled, 32 scans
14 11:38:37 2602121057-0-14-r27389ac 10 PROTON ug2023 + + - + + + + NC W2 crude || 1H Experiment
13 11:32:31 2602121056-0-13-t29189mm 10 PROTON ug2023 + + - + + + + alcohol G || 1H Experiment
11 11:29:39 2602121054-0-11-w75830yw 11 C13CPD32 ug2023 - + - - - + + crude OMe || 13C Experiment, 1H decoupled, 32 scans
11 11:22:58 2602121054-0-11-w75830yw 10 PROTON ug2023 + + - + + + + crude OMe || 1H Experiment
10 11:20:01 2602121052-0-10-t68773xz 11 C13CPD32 ug2023 - + - - - + + XZ_G4_P1-2-2.12 || 13C Experiment, 1H decoupled, 32 scans
10 11:13:50 2602121052-0-10-t68773xz 10 PROTON ug2023 + + - + + + + XZ_G4_P1-2-2.12 || 1H Experiment
9 11:10:54 2602121051-0-9-m61564jh 11 C13CPD32 ug2023 - + - - - + + JQ01_CP_2 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602121051-0-9-m61564jh/11/pdata/1/peaks No peaks found in the specified range.
9 11:03:38 2602121051-0-9-m61564jh 10 PROTON ug2023 + + - + + + + JQ01_CP_2 || 1H Experiment
7 10:59:59 2602121024-0-7-c68704nm 11 C13CPD32 ug2023 - + - - - + + Dini Part1_2 || 13C Experiment, 1H decoupled, 32 scans
7 10:54:42 2602121024-0-7-c68704nm 10 PROTON ug2023 + + - + + + + Dini Part1_2 || 1H Experiment
6 10:52:36 2602121023-0-6-g14620tl 12 P31 ug2023 - + - - - + + PSI REAGENT NMR || 31P Experiment, No Decoupling, 32 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0
6 10:50:20 2602121023-0-6-g14620tl 11 P31CPD ug2023 - + - - - + + PSI REAGENT NMR || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0
6 10:43:14 2602121023-0-6-g14620tl 10 PROTON ug2023 + + - + + + + PSI REAGENT NMR || 1H Experiment
5 10:40:21 2602121019-0-5-p00146sh 11 C13CPD32 ug2023 - + - - - + + Ruogu Final Product amide || 13C Experiment, 1H decoupled, 32 scans
5 10:33:42 2602121019-0-5-p00146sh 10 PROTON ug2023 + + - + + + + Ruogu Final Product amide || 1H Experiment
4 10:30:08 2602121019-0-4-p00146sh 11 C13CPD32 ug2023 - + - - - + + Sam Crude product amide || 13C Experiment, 1H decoupled, 32 scans
4 10:23:49 2602121019-0-4-p00146sh 10 PROTON ug2023 + + - + + + + Sam Crude product amide || 1H Experiment
3 10:21:57 2602121012-0-3-r36807jm 11 F19 ug2023 - + - - - + + n-tert-butyl amide || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
3 10:13:39 2602121012-0-3-r36807jm 10 PROTON ug2023 + + - + + + + n-tert-butyl amide || 1H Experiment
2 16:59:03 2602111036-0-2-k85678ee 10 PROTON ug2024 + + - + + + + EXP14.EE || 1H Experiment
1 16:50:57 2602111028-0-1-p24563cr 10 PROTON ug2024 + + - + + + + CRW.product || 1H Experiment
4 12:04:23 2602111046-0-4-f38977ec 10 PROTON ug2024 + + - + + + + ellieconnerepoxide || 1H Experiment
3 11:57:47 2602111042-0-3-s16700ml 10 PROTON ug2024 + + - + + + + Mhairi Low || 1H Experiment
17 11:49:16 2602111107-0-17-x97127ab 10 PROTON ug2024 + + - + + + + ABProduct || 1H Experiment
16 11:40:27 2602111107-0-16-x97127ab 10 PROTON ug2024 + + - + + + + JKProduct || 1H Experiment
15 11:31:55 2602111041-0-15-p24563cr 10 PROTON ug2024 + + - + + + + CB.pro || 1H Experiment
13 11:25:13 2602111041-0-13-p24563cr 10 PROTON ug2024 + + - + + + + TS.pro || 1H Experiment
12 11:19:02 2602111041-0-12-p24563cr 10 PROTON ug2024 + + - + + + + CRW.pr || 1H Experiment
11 11:11:46 2602111107-0-11-x97127ab 10 PROTON ug2024 + + - + + + + CPProduct || 1H Experiment
18 11:10:39 2602111109-0-18-p62390kt 10 PROTON ug2024 x - - - - - - KTExp14 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
10 11:03:51 2602111057-0-10-j01915sa 10 PROTON ug2024 + + - + + + + ring-open epo || 1H Experiment
5 10:55:55 2602111053-0-5-s99458cg 10 PROTON ug2024 + + - + + + + epoxide ring opening || 1H Experiment
14 08:25:11 2602101523-0-14-n95277os 10 PROTON ug2024 x - - - - - - OS Exp 4 || 1H Experiment SampleChanger Error: 1000 SampleTransportController: No Sample at requested Position.
9 08:18:10 2602101504-0-9-e75990zm 10 PROTON ug2024 + + - + + + + Zara_exp4 || 1H Experiment
8 08:11:29 2602101446-0-8-x89757cd 10 PROTON ug2024 + + - + + + + Carmen || 1H Experiment
7 08:04:50 2602101446-0-7-x89757cd 10 PROTON ug2024 + + - + + + + Eva L || 1H Experiment
6 07:58:54 2602101446-0-6-x89757cd 10 PROTON ug2024 + + - + + + + Isaac || 1H Experiment
5 22:05:12 2602101435-0-5-j78081qc 13 HMBCLPND ug2024 + + - + + + + Exp_4_Cross_Coupling_NMR || Long range 1H-13C correlation
4 21:49:25 2602101432-0-4-h14891yx 14 HSQCEDETGP ug2024 - + - - - + + xiaoyixuan || 1-bond 1H-13C correlation with CH/CH3 up and CH2 down
4 19:47:12 2602101432-0-4-h14891yx 13 HMBCLPND ug2024 - + - - - + + xiaoyixuan || Long range 1H-13C correlation
4 19:41:05 2602101432-0-4-h14891yx 12 COSYGPSW ug2024 - + - - - + + xiaoyixuan || COSY
4 19:38:14 2602101432-0-4-h14891yx 11 C13CPD32 ug2024 - + - - - + + xiaoyixuan || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602101432-0-4-h14891yx/11/pdata/1/peaks No peaks found in the specified range.
4 19:29:50 2602101432-0-4-h14891yx 10 PROTON ug2024 + + - + + + + xiaoyixuan || 1H Experiment
3 17:23:38 2602101430-0-3-z33573yc 13 HMBCLPND ug2024 + + - + + + + Caiyt || Long range 1H-13C correlation
2 16:12:05 2602101337-0-2-mbdssmh7 11 C13CPD teaching + + - + + + + MJH_Y1_Ketal || 13C Experiment, 1H decoupled, 128 scans
16 16:09:12 2602101533-0-16-r75977ma 11 C13CPD32 ug2024 - + - - - + + TAExp4 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602101533-0-16-r75977ma/11/pdata/1/peaks No peaks found in the specified range.
16 16:00:39 2602101533-0-16-r75977ma 10 PROTON ug2024 + + - + + + + TAExp4 || 1H Experiment
12 15:57:50 2602101520-0-12-n95277os 11 PROTON ug2024 - + - - - + + OS Exp 4 || 1H Experiment
12 15:49:19 2602101520-0-12-n95277os 10 C13CPD32 ug2024 + + - + + + + OS Exp 4 || 13C Experiment, 1H decoupled, 32 scans
15 15:46:25 2602101527-0-15-k72170ys 11 C13CPD32 ug2024 - + - - - + + suzy1 || 13C Experiment, 1H decoupled, 32 scans
15 15:39:48 2602101527-0-15-k72170ys 10 PROTON ug2024 + + - + + + + suzy1 || 1H Experiment
13 15:36:52 2602101525-0-13-r75977ma 11 C13CPD32 ug2024 - + - - - + + MAL EXP 4 || 13C Experiment, 1H decoupled, 32 scans
13 15:30:00 2602101525-0-13-r75977ma 10 PROTON ug2024 + + - + + + + MAL EXP 4 || 1H Experiment
11 15:19:36 2602101511-0-11-z78389zo 10 PROTON ug2024 + + - + + + + zacksiv || 1H Experiment
10 15:12:30 2602101511-0-10-z78389zo 10 PROTON ug2024 + + - + + + + kpottelol || 1H Experiment
5 15:02:40 2602101435-0-5-j78081qc 12 COSYGPSW ug2024 - + - - - + + Exp_4_Cross_Coupling_NMR || COSY
5 14:59:47 2602101435-0-5-j78081qc 11 C13CPD32 ug2024 - + - - - + + Exp_4_Cross_Coupling_NMR || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602101435-0-5-j78081qc/11/pdata/1/peaks No peaks found in the specified range.
5 14:49:27 2602101435-0-5-j78081qc 10 PROTON ug2024 + + - + + + + Exp_4_Cross_Coupling_NMR || 1H Experiment
3 14:43:18 2602101430-0-3-z33573yc 12 COSYGPSW ug2024 - + - - - + + Caiyt || COSY
3 14:40:27 2602101430-0-3-z33573yc 11 C13CPD32 ug2024 - + - - - + + Caiyt || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602101430-0-3-z33573yc/11/pdata/1/peaks No peaks found in the specified range.
3 14:34:58 2602101430-0-3-z33573yc 10 PROTON ug2024 + + - + + + + Caiyt || 1H Experiment
2 14:25:05 2602101337-0-2-mbdssmh7 10 PROTON teaching + + - + + + + MJH_Y1_Ketal || 1H Experiment
1 13:14:03 2602101130-0-1-mbdssmh7 11 C13CPD teaching + + - + + + + MJH_Y1_SalenH2 || 13C Experiment, 1H decoupled, 128 scans
1 11:32:45 2602101130-0-1-mbdssmh7 10 PROTON teaching + + - + + + + MJH_Y1_SalenH2 || 1H Experiment
56 01:35:57 2602061114-0-56-p12908lh 11 C13CPD32 ug2023 - + - - - + + Con-TPGS-750-M Prod. || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602061114-0-56-p12908lh/11/pdata/1/peaks No peaks found in the specified range.
56 01:28:19 2602061114-0-56-p12908lh 10 PROTON ug2023 + + - + + + + Con-TPGS-750-M Prod. || 1H Experiment
55 01:25:25 2602061114-0-55-p12908lh 11 C13CPD32 ug2023 - + - - - + + Dis-TPGS-750-M Prod. || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602061114-0-55-p12908lh/11/pdata/1/peaks No peaks found in the specified range.
55 01:19:12 2602061114-0-55-p12908lh 10 PROTON ug2023 + + - + + + + Dis-TPGS-750-M Prod. || 1H Experiment
53 01:18:49 2602061413-0-53-r36807jm 10 PROTON ug2023 x - - - - - - Jood Pre Column || 1H Experiment SampleChanger Error: 1000 SampleTransportController: No Sample at requested Position.
33 01:10:21 2602091507-0-33-v96919bm 10 PROTON ug2025 + + - + + + + experiment14-Fe || 1H Experiment
32 01:04:08 2602091505-0-32-z19309wz 10 PROTON ug2025 + + - + + + + EXP2 WZ || 1H Experiment
31 00:55:48 2602091511-0-31-v96919bm 10 PROTON ug2025 + + - + + + + experiment14-NaBH4 || 1H Experiment
12 00:53:05 20260209-1121-B300_2.044-12 13 PROTON y1-K/E - + - - - + + Ref ace.one 4
12 00:50:22 20260209-1121-B300_2.044-12 12 PROTON y1-K/E - + - - - + + Ref ace.one 3
12 00:47:39 20260209-1121-B300_2.044-12 11 PROTON y1-K/E - + - - - + + Ref ace.one 2
12 00:40:21 20260209-1121-B300_2.044-12 10 PROTON y1-K/E + + - + + + + Ref ace.one 1
6 00:37:44 20260209-1107-B300_2.044-6 13 PROTON y1-K/E - + - - - + + Ref James-ethyl t4
6 00:35:07 20260209-1107-B300_2.044-6 12 PROTON y1-K/E - + - - - + + Ref James-ethyl t3
6 00:32:29 20260209-1107-B300_2.044-6 11 PROTON y1-K/E - + - - - + + Ref James-ethyl t2
6 00:25:31 20260209-1107-B300_2.044-6 10 PROTON y1-K/E + + - + + + + Ref James-ethyl t1
5 00:22:54 20260209-1112-B300_2.044-5 13 PROTON y1-K/E - + - - - + + Ref James -acetyl t4
5 00:20:09 20260209-1112-B300_2.044-5 12 PROTON y1-K/E - + - - - + + Ref James -acetyl t3
5 00:17:32 20260209-1112-B300_2.044-5 11 PROTON y1-K/E - + - - - + + Ref James -acetyl t2
5 00:09:49 20260209-1112-B300_2.044-5 10 PROTON y1-K/E + + - + + + + Ref James -acetyl t1
11 00:07:04 20260209-1117-B300_2.044-11 13 PROTON y1-K/E - + - - - + + Ref ate t4
11 00:00:43 20260209-1117-B300_2.044-11 12 PROTON y1-K/E + + - + + + + Ref ate t3
30 23:54:03 20260209-1143-B300_2.044-30 14 PROTON y1-K/E + + - + + + + Ref phneylbutane 4
29 23:47:52 20260209-1143-B300_2.044-29 13 PROTON y1-K/E + + - + + + + Ref ethyl acetoneacetate 4
28 23:40:48 20260209-1143-B300_2.044-28 13 PROTON y1-K/E + + - + + + + Ref Acetylacetone 4
27 23:34:07 20260209-1137-B300_2.044-27 13 PROTON y1-K/E + + - + + + + Ref Ethyl 4
26 23:27:09 20260209-1137-B300_2.044-26 13 PROTON y1-K/E + + - + + + + Ref Acetyl 4
25 23:19:28 20260209-1137-B300_2.044-25 13 PROTON y1-K/E + + - + + + + Ref phenyl 4
24 23:13:24 20260209-1133-B300_2.044-24 13 PROTON y1-K/E + + - + + + + Ref 1-P 4
23 23:07:11 20260209-1133-B300_2.044-23 13 PROTON y1-K/E + + - + + + + Ref aa 4
22 23:01:02 20260209-1133-B300_2.044-22 13 PROTON y1-K/E + + - + + + + Ref ea 4
21 22:54:19 20260209-1129-B300_2.044-21 13 PROTON y1-K/E + + - + + + + Ref Phenyl 4
19 22:47:37 20260209-1129-B300_2.044-19 13 PROTON y1-K/E + + - + + + + Ref Acetylacetone 4
18 22:41:04 20260209-1125-B300_2.044-18 13 PROTON y1-K/E + + - + + + + Ref Phenyl butadione 4
17 22:32:35 20260209-1125-B300_2.044-17 13 PROTON y1-K/E + + - + + + + Ref Acetylacetone 4
16 22:25:08 20260209-1125-B300_2.044-16 13 PROTON y1-K/E + + - + + + + Ref ethyl acetoneacetate 4
15 22:19:22 20260209-1121-B300_2.044-15 13 PROTON y1-K/E + + - + + + + Ref Ace 4
14 22:13:06 20260209-1121-B300_2.044-14 13 PROTON y1-K/E + + - + + + + Ref 1,3 4
13 22:00:18 20260209-1121-B300_2.044-13 13 PROTON y1-K/E + + - + + + + Ref Ethyl 4
20 21:52:27 20260209-1129-B300_2.044-20 13 PROTON y1-K/E + + - + + + + Ref Ethyl 4
10 21:45:47 20260209-1117-B300_2.044-10 13 PROTON y1-K/E + + - + + + + Ref 1,3-dione t4
9 21:38:09 20260209-1113-B300_2.044-9 13 PROTON y1-K/E + + - + + + + Ref Phenyl t4
8 21:29:34 20260209-1113-B300_2.044-8 13 PROTON y1-K/E + + - + + + + Ref ethyl t4
30 21:21:59 20260209-1143-B300_2.044-30 12 PROTON y1-K/E + + - + + + + Ref phneylbutane 3
7 21:14:40 20260209-1113-B300_2.044-7 13 PROTON y1-K/E + + - + + + + Ref Acetyl t4
29 21:08:01 20260209-1143-B300_2.044-29 12 PROTON y1-K/E + + - + + + + Ref ethyl acetoneacetate 3
28 20:59:03 20260209-1143-B300_2.044-28 12 PROTON y1-K/E + + - + + + + Ref Acetylacetone 3
27 20:50:40 20260209-1137-B300_2.044-27 12 PROTON y1-K/E + + - + + + + Ref Ethyl 3
26 20:42:22 20260209-1137-B300_2.044-26 12 PROTON y1-K/E + + - + + + + Ref Acetyl 3
4 20:35:54 20260209-1107-B300_2.044-4 13 PROTON y1-K/E + + - + + + + Ref james-phenyl
25 20:29:35 20260209-1137-B300_2.044-25 12 PROTON y1-K/E + + - + + + + Ref phenyl 3
24 20:23:00 20260209-1133-B300_2.044-24 12 PROTON y1-K/E + + - + + + + Ref 1-P 3
23 20:16:15 20260209-1133-B300_2.044-23 12 PROTON y1-K/E + + - + + + + Ref aa 3
22 20:10:12 20260209-1133-B300_2.044-22 12 PROTON y1-K/E + + - + + + + Ref ea 3
21 20:03:57 20260209-1129-B300_2.044-21 12 PROTON y1-K/E + + - + + + + Ref Phenyl 3
20 19:54:00 20260209-1129-B300_2.044-20 12 PROTON y1-K/E + + - + + + + Ref Ethyl 3
3 19:46:36 20260209-1057-B300_2.044-3 13 PROTON y1-K/E + + - + + + + Ref NS-P t4
19 19:40:26 20260209-1129-B300_2.044-19 12 PROTON y1-K/E + + - + + + + Ref Acetylacetone 3
18 19:31:23 20260209-1125-B300_2.044-18 12 PROTON y1-K/E + + - + + + + Ref Phenyl butadione 3
2 19:23:17 20260209-1056-B300_2.044-2 13 PROTON y1-K/E + + - + + + + Ref NS-E T4
17 19:17:08 20260209-1125-B300_2.044-17 12 PROTON y1-K/E + + - + + + + Ref Acetylacetone 3
16 19:08:13 20260209-1125-B300_2.044-16 12 PROTON y1-K/E + + - + + + + Ref ethyl acetoneacetate 3
1 19:01:55 20260209-1052-B300_2.044-1 13 PROTON y1-K/E + + - + + + + Ref NS-A t4
15 18:54:49 20260209-1121-B300_2.044-15 12 PROTON y1-K/E + + - + + + + Ref Ace 3
14 18:48:38 20260209-1121-B300_2.044-14 12 PROTON y1-K/E + + - + + + + Ref 1,3 3
13 18:36:56 20260209-1121-B300_2.044-13 12 PROTON y1-K/E + + - + + + + Ref Ethyl 3
10 18:30:44 20260209-1117-B300_2.044-10 12 PROTON y1-K/E + + - + + + + Ref 1,3-dione t3
9 18:24:35 20260209-1113-B300_2.044-9 12 PROTON y1-K/E + + - + + + + Ref Phenyl t3
8 18:17:50 20260209-1113-B300_2.044-8 12 PROTON y1-K/E + + - + + + + Ref ethyl t3
30 18:09:21 20260209-1143-B300_2.044-30 11 PROTON y1-K/E + + - + + + + Ref phneylbutane 2
7 18:00:46 20260209-1113-B300_2.044-7 12 PROTON y1-K/E + + - + + + + Ref Acetyl t3
29 17:54:35 20260209-1143-B300_2.044-29 11 PROTON y1-K/E + + - + + + + Ref ethyl acetoneacetate 2
28 17:47:54 20260209-1143-B300_2.044-28 11 PROTON y1-K/E + + - + + + + Ref Acetylacetone 2
27 17:40:46 20260209-1137-B300_2.044-27 11 PROTON y1-K/E + + - + + + + Ref Ethyl 2
26 17:33:48 20260209-1137-B300_2.044-26 11 PROTON y1-K/E + + - + + + + Ref Acetyl 2
4 17:25:36 20260209-1107-B300_2.044-4 12 PROTON y1-K/E + + - + + + + Ref james-phenyl
25 17:19:18 20260209-1137-B300_2.044-25 11 PROTON y1-K/E + + - + + + + Ref phenyl 2
24 17:11:57 20260209-1133-B300_2.044-24 11 PROTON y1-K/E + + - + + + + Ref 1-P 2
23 17:05:18 20260209-1133-B300_2.044-23 11 PROTON y1-K/E + + - + + + + Ref aa 2
22 16:57:44 20260209-1133-B300_2.044-22 11 PROTON y1-K/E + + - + + + + Ref ea 2
21 16:51:27 20260209-1129-B300_2.044-21 11 PROTON y1-K/E + + - + + + + Ref Phenyl 2
20 16:44:49 20260209-1129-B300_2.044-20 11 PROTON y1-K/E + + - + + + + Ref Ethyl 2
19 16:37:12 20260209-1129-B300_2.044-19 11 PROTON y1-K/E + + - + + + + Ref Acetylacetone 2
3 16:30:15 20260209-1057-B300_2.044-3 12 PROTON y1-K/E + + - + + + + Ref NS-P t3
18 16:21:16 20260209-1125-B300_2.044-18 11 PROTON y1-K/E + + - + + + + Ref Phenyl butadione 2
2 16:15:26 20260209-1056-B300_2.044-2 12 PROTON y1-K/E + + - + + + + Ref NS-E T3
17 16:08:49 20260209-1125-B300_2.044-17 11 PROTON y1-K/E + + - + + + + Ref Acetylacetone 2
16 16:02:07 20260209-1125-B300_2.044-16 11 PROTON y1-K/E + + - + + + + Ref ethyl acetoneacetate 2
1 15:53:35 20260209-1052-B300_2.044-1 12 PROTON y1-K/E + + - + + + + Ref NS-A t3
15 15:45:33 20260209-1121-B300_2.044-15 11 PROTON y1-K/E + + - + + + + Ref Ace 2
14 15:39:19 20260209-1121-B300_2.044-14 11 PROTON y1-K/E + + - + + + + Ref 1,3 2
13 15:27:11 20260209-1121-B300_2.044-13 11 PROTON y1-K/E + + - + + + + Ref Ethyl 2
11 15:18:42 20260209-1117-B300_2.044-11 11 PROTON y1-K/E + + - + + + + Ref ate t2
10 15:11:55 20260209-1117-B300_2.044-10 11 PROTON y1-K/E + + - + + + + Ref 1,3-dione t2
30 15:02:39 20260209-1143-B300_2.044-30 10 PROTON y1-K/E + + - + + + + Ref phneylbutane 1
9 14:56:22 20260209-1113-B300_2.044-9 11 PROTON y1-K/E + + - + + + + Ref Phenyl t2
8 14:50:05 20260209-1113-B300_2.044-8 11 PROTON y1-K/E + + - + + + + Ref ethyl t2
29 14:41:09 20260209-1143-B300_2.044-29 10 PROTON y1-K/E + + - + + + + Ref ethyl acetoneacetate 1
7 14:33:57 20260209-1113-B300_2.044-7 11 PROTON y1-K/E + + - + + + + Ref Acetyl t2
28 14:27:15 20260209-1143-B300_2.044-28 10 PROTON y1-K/E + + - + + + + Ref Acetylacetone 1
27 14:21:09 20260209-1137-B300_2.044-27 10 PROTON y1-K/E + + - + + + + Ref Ethyl 1
26 14:14:33 20260209-1137-B300_2.044-26 10 PROTON y1-K/E + + - + + + + Ref Acetyl 1
25 14:04:45 20260209-1137-B300_2.044-25 10 PROTON y1-K/E + + - + + + + Ref phenyl 1
4 13:57:34 20260209-1107-B300_2.044-4 11 PROTON y1-K/E + + - + + + + Ref james-phenyl
24 13:50:23 20260209-1133-B300_2.044-24 10 PROTON y1-K/E + + - + + + + Ref 1-P 1
23 13:43:13 20260209-1133-B300_2.044-23 10 PROTON y1-K/E + + - + + + + Ref aa 1
22 13:36:38 20260209-1133-B300_2.044-22 10 PROTON y1-K/E + + - + + + + Ref ea 1
21 13:29:02 20260209-1129-B300_2.044-21 10 PROTON y1-K/E + + - + + + + Ref Phenyl 1
20 13:22:46 20260209-1129-B300_2.044-20 10 PROTON y1-K/E + + - + + + + Ref Ethyl 1
19 13:16:33 20260209-1129-B300_2.044-19 10 PROTON y1-K/E + + - + + + + Ref Acetylacetone 1
18 13:07:35 20260209-1125-B300_2.044-18 10 PROTON y1-K/E + + - + + + + Ref Phenyl butadione 1
3 13:00:11 20260209-1057-B300_2.044-3 11 PROTON y1-K/E + + - + + + + Ref NS-P t2
17 12:53:25 20260209-1125-B300_2.044-17 10 PROTON y1-K/E + + - + + + + Ref Acetylacetone 1
16 12:45:03 20260209-1125-B300_2.044-16 10 PROTON y1-K/E + + - + + + + Ref ethyl acetoneacetate 1
2 12:35:40 20260209-1056-B300_2.044-2 11 PROTON y1-K/E + + - + + + + Ref NS-E T2
1 12:27:07 20260209-1052-B300_2.044-1 11 PROTON y1-K/E + + - + + + + Ref NS-A t2
15 12:20:50 20260209-1121-B300_2.044-15 10 PROTON y1-K/E + + - + + + + Ref Ace 1
14 12:14:10 20260209-1121-B300_2.044-14 10 PROTON y1-K/E + + - + + + + Ref 1,3 1
13 12:07:03 20260209-1121-B300_2.044-13 10 PROTON y1-K/E + + - + + + + Ref Ethyl 1
11 11:59:03 20260209-1117-B300_2.044-11 10 PROTON y1-K/E + + - + + + + Ref ate t1
10 11:50:11 20260209-1117-B300_2.044-10 10 PROTON y1-K/E + + - + + + + Ref 1,3-dione t1
9 11:41:14 20260209-1113-B300_2.044-9 10 PROTON y1-K/E + + - + + + + Ref Phenyl t1
8 11:35:04 20260209-1113-B300_2.044-8 10 PROTON y1-K/E + + - + + + + Ref ethyl t1
7 11:27:52 20260209-1113-B300_2.044-7 10 PROTON y1-K/E + + - + + + + Ref Acetyl t1
4 11:19:56 20260209-1107-B300_2.044-4 10 PROTON y1-K/E + + - + + + + Ref james-phenyl
3 11:13:43 20260209-1057-B300_2.044-3 10 PROTON y1-K/E + + - + + + + Ref NS-P t1
2 11:07:18 20260209-1056-B300_2.044-2 10 PROTON y1-K/E + + - + + + + Ref NS-E T1
1 11:00:26 20260209-1052-B300_2.044-1 10 PROTON y1-K/E + + - + + + + Ref NS-A t1
60 16:06:06 2602061418-0-60-b93379br 11 C13CPD32 ug2023 - + - - - + + Lee Pre Column || 13C Experiment, 1H decoupled, 32 scans
60 15:58:52 2602061418-0-60-b93379br 10 PROTON ug2023 + + - + + + + Lee Pre Column || 1H Experiment
59 15:55:53 2602061418-0-59-b93379br 11 C13CPD32 ug2023 - + - - - + + Jood Pre Column || 13C Experiment, 1H decoupled, 32 scans
59 15:48:26 2602061418-0-59-b93379br 10 PROTON ug2023 + + - + + + + Jood Pre Column || 1H Experiment
22 04:06:06 2602061535-0-22-z73813ns 10 PROTON ug2023 + + - + + + + Carbodiimine D 1H || 1H Experiment
58 03:57:27 2602061547-0-58-d98689cd 10 PROTON ug2023 + + - + + + + Anisole || 1H Experiment
54 03:48:47 2602061547-0-54-d98689cd 10 PROTON ug2023 + + - + + + + Solid || 1H Experiment
51 03:42:03 2602061547-0-51-d98689cd 10 PROTON ug2023 + + - + + + + HAG32 || 1H Experiment
39 03:33:47 2602061547-0-39-d98689cd 10 PROTON ug2023 + + - + + + + ISG32 || 1H Experiment
38 03:30:47 2602061544-0-38-k03256gd 11 C13CPD32 ug2023 - + - - - + + Filtrate || 13C Experiment, 1H decoupled, 32 scans
38 03:25:04 2602061544-0-38-k03256gd 10 PROTON ug2023 + + - + + + + Filtrate || 1H Experiment
37 03:22:00 2602061544-0-37-k03256gd 11 C13CPD32 ug2023 - + - - - + + Amine B || 13C Experiment, 1H decoupled, 32 scans
37 03:15:45 2602061544-0-37-k03256gd 10 PROTON ug2023 + + - + + + + Amine B || 1H Experiment
21 03:09:32 2602061534-0-21-d98689cd 10 PROTON ug2023 + + - + + + + G32 Coupling Product || 1H Experiment
3 03:02:03 2602061527-0-3-t69807al 10 PROTON ug2023 + + - + + + + carbodiimide A || 1H Experiment
19 02:55:02 2602061534-0-19-n98843hm 10 PROTON ug2023 + + - + + + + morpholine_90*C_40mins_pg37 || 1H Experiment
18 02:46:03 2602061531-0-18-t19785ak 10 PROTON ug2023 + + - + + + + Anees 4-ep water 90 degrees || 1H Experiment
17 02:34:11 2602061531-0-17-t19785ak 10 PROTON ug2023 + + - + + + + Billy azep[ane water m,edium 90 bdegrees || 1H Experiment
16 02:29:01 2602061528-0-16-d37549ac 10 PROTON ug2023 + + - + + + + product first part || 1H Experiment
15 02:25:53 2602061523-0-15-k03256gd 11 C13CPD32 ug2023 - + - - - + + Crude carbodiimide C || 13C Experiment, 1H decoupled, 32 scans
15 02:19:59 2602061523-0-15-k03256gd 10 PROTON ug2023 + + - + + + + Crude carbodiimide C || 1H Experiment
12 02:11:58 2602061515-0-12-q09060yz 10 PROTON ug2023 + + - + + + + etoh 3:1 zyeee b || 1H Experiment
11 02:06:05 2602061515-0-11-q09060yz 10 PROTON ug2023 + + - + + + + etoh 2:1 zyeee a || 1H Experiment
9 02:03:11 2602061512-0-9-w75830yw 11 C13CPD32 ug2023 - + - - - + + crude ome || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602061512-0-9-w75830yw/11/pdata/1/peaks No peaks found in the specified range.
9 01:56:43 2602061512-0-9-w75830yw 10 PROTON ug2023 + + - + + + + crude ome || 1H Experiment
10 01:53:49 2602061513-0-10-t68773xz 11 C13CPD32 ug2023 - + - - - + + XZ_G4_F-_P1 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602061513-0-10-t68773xz/11/pdata/1/peaks No peaks found in the specified range.
10 01:48:04 2602061513-0-10-t68773xz 10 PROTON ug2023 + + - + + + + XZ_G4_F-_P1 || 1H Experiment
7 01:45:10 2602061511-0-7-m61564jh 11 C13CPD32 ug2023 - + - - - + + JQ_01_P || 13C Experiment, 1H decoupled, 32 scans
7 01:39:05 2602061511-0-7-m61564jh 10 PROTON ug2023 + + - + + + + JQ_01_P || 1H Experiment
8 01:36:10 2602061511-0-8-r27389ac 11 C13CPD32 ug2023 - + - - - + + NC crude prod || 13C Experiment, 1H decoupled, 32 scans
8 01:31:00 2602061511-0-8-r27389ac 10 PROTON ug2023 + + - + + + + NC crude prod || 1H Experiment
6 01:24:18 2602061507-0-6-y12416yo 10 PROTON ug2023 + + - + + + + yj.terpinene.g12 || 1H Experiment
5 01:17:42 2602061507-0-5-d96985hs 10 PROTON ug2023 + + - + + + + Friday Week 1 4-nitro benzaldehyde HS || 1H Experiment
4 01:10:34 2602061507-0-4-d96985hs 10 PROTON ug2023 + + - + + + + Friday Week 1 isobutryaldehyde HS || 1H Experiment
2 01:04:09 2602061441-0-2-t19785ak 10 PROTON ug2023 + + - + + + + 4-ep water solvent sample 2 smalleer pure sample || 1H Experiment
1 00:51:09 2602061441-0-1-t19785ak 10 PROTON ug2023 + + - + + + + 4-ethyllpiperazine under 90 degrees water medium sample 1 || 1H Experiment
50 00:44:11 2602061356-0-50-z34413sw 10 PROTON ug2023 + + - + + + + G14-AK2 || 1H Experiment
46 23:36:46 2602061336-0-46-a28784zr 11 C13CPD ug2023 - + - - - + + Exp4 t24 || 13C Experiment, 1H decoupled, 128 scans
46 23:30:35 2602061336-0-46-a28784zr 10 PROTON ug2023 + + - + + + + Exp4 t24 || 1H Experiment
45 22:23:10 2602061336-0-45-a28784zr 11 C13CPD ug2023 - + - - - + + DMF 38 || 13C Experiment, 1H decoupled, 128 scans
45 22:16:01 2602061336-0-45-a28784zr 10 PROTON ug2023 + + - + + + + DMF 38 || 1H Experiment
44 21:08:39 2602061336-0-44-a28784zr 11 C13CPD ug2023 - + - - - + + 38 THF || 13C Experiment, 1H decoupled, 128 scans
44 21:02:02 2602061336-0-44-a28784zr 10 PROTON ug2023 + + - + + + + 38 THF || 1H Experiment
43 19:54:38 2602061336-0-43-a28784zr 11 C13CPD ug2023 - + - - - + + 38 N+233 || 13C Experiment, 1H decoupled, 128 scans
43 19:47:08 2602061336-0-43-a28784zr 10 PROTON ug2023 + + - + + + + 38 N+233 || 1H Experiment
42 18:39:36 2602061336-0-42-a28784zr 11 C13CPD ug2023 - + - - - + + S3.38 || 13C Experiment, 1H decoupled, 128 scans
42 18:31:42 2602061336-0-42-a28784zr 10 PROTON ug2023 + + - + + + + S3.38 || 1H Experiment
49 18:28:48 2602061325-0-49-r27389ac 11 C13CPD32 ug2023 - + - - - + + AC reagent || 13C Experiment, 1H decoupled, 32 scans
49 18:23:31 2602061325-0-49-r27389ac 10 PROTON ug2023 + + - + + + + AC reagent || 1H Experiment
48 18:20:39 2602061325-0-48-r27389ac 11 C13CPD32 ug2023 - + - - - + + NC reagent || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602061325-0-48-r27389ac/11/pdata/1/peaks No peaks found in the specified range.
48 18:15:12 2602061325-0-48-r27389ac 10 PROTON ug2023 + + - + + + + NC reagent || 1H Experiment
41 18:07:43 2602061320-0-41-j85765wh 10 PROTON ug2023 + + - + + + + PiperideneRM || 1H Experiment
40 17:56:33 2602061320-0-40-j85765wh 10 PROTON ug2023 + + - + + + + MorpholineRM || 1H Experiment
47 17:55:31 2602061319-0-47-w75830yw 10 PROTON ug2023 x - - - - - - ome starting || 1H Experiment SampleChanger Error: 1000 SampleTransportController: No Sample at requested Position.
52 17:47:55 2602061317-0-52-a98524wr 10 PROTON ug2023 + + - + + + + Knoevenagel adduct for propanal, JMM || 1H Experiment
34 17:42:25 2602061312-0-34-c68402hw 11 C13CPD32 ug2023 - + - - - + + Urea B concentrated || 13C Experiment, 1H decoupled, 32 scans
34 17:36:24 2602061312-0-34-c68402hw 10 PROTON ug2023 + + - + + + + Urea B concentrated || 1H Experiment
36 17:30:12 2602061313-0-36-a98524wr 10 PROTON ug2023 + + - + + + + Will Week 1 Friday Reaction 2 Benzaldehyde (1:1.1) || 1H Experiment
35 17:23:51 2602061313-0-35-a98524wr 10 PROTON ug2023 + + - + + + + Will Week 1 Friday Reaction 1 Benzaldehyde (1:2.2) || 1H Experiment
33 17:16:51 2602061311-0-33-p00146sh 11 C13CPD32 ug2023 + + - + + + + o-toluoyl chloride starting material G30 || 13C Experiment, 1H decoupled, 32 scans
20 16:05:13 2602061249-0-20-g14620tl 13 C13CPD ug2023 + + - + + + + Thiophosphate crude NMR || 13C Experiment, 1H decoupled, 128 scans
33 15:59:06 2602061311-0-33-p00146sh 10 PROTON ug2023 + + - + + + + o-toluoyl chloride starting material G30 || 1H Experiment
32 15:53:21 2602061307-0-32-d98689cd 10 PROTON ug2023 + + - + + + + CD coupling product || 1H Experiment
31 15:44:49 2602061306-0-31-d94069rz 10 PROTON ug2023 + + - + + + + crude || 1H Experiment
30 15:36:51 2602061306-0-30-d94069rz 10 PROTON ug2023 + + - + + + + starting || 1H Experiment
29 15:31:10 2602061258-0-29-k21450ms 10 PROTON ug2023 + + - + + + + MS-thread 3 || 1H Experiment
28 15:25:30 2602061258-0-28-k21450ms 10 PROTON ug2023 + + - + + + + RN-thread 3 || 1H Experiment
27 15:17:04 2602061253-0-27-r99959zh 10 PROTON ug2023 + + - + + + + G3 FEE || 1H Experiment
26 15:10:25 2602061257-0-26-a98524wr 10 PROTON ug2023 + + - + + + + King-Jerry, Week 1, Friday, Knoevenagel-Michael Final Product, Hexanal || 1H Experiment
25 15:02:43 2602061257-0-25-a98524wr 10 PROTON ug2023 + + - + + + + King-Jerry, Week 1, Friday, Knoevenagel-Michael 40 mins in, Hexanal || 1H Experiment
24 14:55:31 2602061257-0-24-a98524wr 10 PROTON ug2023 + + - + + + + King-Jerry, Week 1, Friday, Knoevenagel-Michael 30 mins in, Hexanal || 1H Experiment
23 14:49:19 2602061257-0-23-a98524wr 10 PROTON ug2023 + + - + + + + King-Jerry, Week1, Friday, Knoevenagel-Michael 20 mins in, Hexanal || 1H Experiment
21 14:43:08 2602061257-0-21-a98524wr 10 PROTON ug2023 + + - + + + + King-Jerry, Week1, Friday, Knoevenagel-Michael 10 mins in, Hexanal || 1H Experiment
20 14:41:00 2602061249-0-20-g14620tl 12 P31 ug2023 - + - - - + + Thiophosphate crude NMR || 31P Experiment, No Decoupling, 32 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0
20 14:38:47 2602061249-0-20-g14620tl 11 P31CPD ug2023 - + - - - + + Thiophosphate crude NMR || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0
20 14:31:09 2602061249-0-20-g14620tl 10 PROTON ug2023 + + - + + + + Thiophosphate crude NMR || 1H Experiment
18 14:25:56 2602061245-0-18-v45005oc 10 PROTON ug2023 + + - + + + + OC Day 1 || 1H Experiment
17 14:22:57 2602061240-0-17-c68704nm 11 C13CPD32 ug2023 - + - - - + + ISOMER Week1_1 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602061240-0-17-c68704nm/11/pdata/1/peaks No peaks found in the specified range.
17 14:17:38 2602061240-0-17-c68704nm 10 PROTON ug2023 + + - + + + + ISOMER Week1_1 || 1H Experiment
16 14:10:07 2602061229-0-16-e10990lb 10 PROTON ug2023 + + - + + + + Benzyl 4-MU Ester Crude || 1H Experiment
15 14:07:12 2602061231-0-15-z91447bd 11 C13CPD32 ug2023 - + - - - + + Crude product 1 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602061231-0-15-z91447bd/11/pdata/1/peaks No peaks found in the specified range.
15 13:59:41 2602061231-0-15-z91447bd 10 PROTON ug2023 + + - + + + + Crude product 1 || 1H Experiment
14 13:56:48 2602061231-0-14-z91447bd 11 C13CPD32 ug2023 - + - - - + + 4-MU starting mat || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602061231-0-14-z91447bd/11/pdata/1/peaks No peaks found in the specified range.
14 13:48:14 2602061231-0-14-z91447bd 10 PROTON ug2023 + + - + + + + 4-MU starting mat || 1H Experiment
13 13:39:51 2602061223-0-13-z34413sw 10 PROTON ug2023 + + - + + + + G14-OMe-2 || 1H Experiment
12 13:33:09 2602061222-0-12-a98524wr 10 PROTON ug2023 + + - + + + + JMM propanal sample, final product from friday || 1H Experiment
11 13:26:47 2602061212-0-11-z73813ns 10 C13CPD32 ug2023 + + - + + + + Urea D 13C || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602061212-0-11-z73813ns/10/pdata/1/peaks No peaks found in the specified range.
10 13:18:41 2602061201-0-10-z34413sw 10 PROTON ug2023 + + - + + + + G14-AK || 1H Experiment
9 13:04:30 2602061201-0-9-z34413sw 10 PROTON ug2023 + + - + + + + G14-OMe || 1H Experiment topshim: waitForThisEvent - lock system status ready : timeout after 30 sec waitForThisEvent - locked in : timeout after 30 sec autoLock - could not lock in successfully, Lock anomaly during acquisition
8 12:55:50 2602061158-0-8-z73813ns 10 PROTON ug2023 + + - + + + + Urea D 1H || 1H Experiment
4 12:50:12 2602061155-0-4-m00673hs 10 PROTON ug2023 + + - + + + + Wildflower2 || 1H Experiment
3 12:44:40 2602061155-0-3-m00673hs 10 PROTON ug2023 + + - + + + + Wildflower1 || 1H Experiment
2 12:38:44 2602061155-0-2-m00673hs 10 PROTON ug2023 + + - + + + + Blank || 1H Experiment
7 11:59:27 2602061156-0-7-s04936gr 10 PROTON ug2023 x - - - - - - manuka3 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
6 11:59:24 2602061156-0-6-s04936gr 10 PROTON ug2023 x - - - - - - manuka2 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
5 11:59:22 2602061156-0-5-s04936gr 10 PROTON ug2023 x - - - - - - manuka1 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
1 11:52:03 2602061141-0-1-a98524wr 10 PROTON ug2023 + + - + + + + JMM time stamp 40 minutes, propanal || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Inconsistent Inputs detected by Controller, please check light barriers. SMCB input word: 0x00011B43
58 11:45:34 2602061117-0-58-a98524wr 10 PROTON ug2023 + + - + + + + JMM time stamp 25 minutes, propanal || 1H Experiment
54 11:38:29 2602061107-0-54-a98524wr 10 PROTON ug2023 + + - + + + + JMM, 10 minute stamp with propanal || 1H Experiment
57 11:21:24 2602061120-0-57-t68773xz 10 PROTON ug2023 x - - - - - - XZ_G4_SM_F || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
60 11:21:21 2602061120-0-60-t68773xz 10 PROTON ug2023 x - - - - - - XZ_G4_Ir || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
59 11:19:01 2602061118-0-59-m61564jh 10 PROTON ug2023 x - - - - - - JQ_01_Cl_SM || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Timeout while trying to rotate. Transport FSM is in unexpected state 34: sample is too high for rotation
53 10:46:16 2602061026-0-53-b35901ws 10 PROTON ug2023 + + - + + + + 20 mins || 1H Experiment
52 10:40:12 2602061026-0-52-b35901ws 10 PROTON ug2023 + + - + + + + 10 mins || 1H Experiment
51 10:32:50 2602061026-0-51-b35901ws 10 PROTON ug2023 + + - + + + + 5 mins || 1H Experiment
50 10:24:50 2602061024-0-50-b35901ws 10 PROTON ug2023 + + - + + + + 2 mins || 1H Experiment
49 08:54:54 2602060813-0-49-mbdssmh7 10 PROTON teaching + + - + + + + Y1_E14_ETOH_6 || 1H Experiment
48 08:48:42 2602060812-0-48-mbdssmh7 10 PROTON teaching + + - + + + + Y1_E14_ETOH_5 || 1H Experiment
47 08:40:28 2602060812-0-47-mbdssmh7 10 PROTON teaching + + - + + + + Y1_E14_ETOH_4 || 1H Experiment
46 08:33:56 2602060812-0-46-mbdssmh7 10 PROTON teaching + + - + + + + Y1_E14_ETOH_3 || 1H Experiment
45 08:28:24 2602060812-0-45-mbdssmh7 10 PROTON teaching + + - + + + + Y1_E14_ETOH_2 || 1H Experiment
44 08:20:24 2602060812-0-44-mbdssmh7 10 PROTON teaching + + - + + + + Y1_E14_ETOH_1 || 1H Experiment
43 08:13:30 2602051526-0-43-r33083aj 10 PROTON ug2023 + + - + + + + Glucaronic acid in chloroform || 1H Experiment
42 18:51:02 2602051509-0-42-t19785ak 10 PROTON ug2023 + + - + + + + 4-vp product || 1H Experiment
41 18:42:03 2602051505-0-41-t29189mm 10 PROTON ug2023 + + - + + + + methoxybenzaldehyde || 1H Experiment
40 18:29:53 2602051505-0-40-t29189mm 10 PROTON ug2023 + + - + + + + methylbenzaldehyde || 1H Experiment
39 18:23:01 2602051505-0-39-t29189mm 10 PROTON ug2023 + + - + + + + 4fluorobenzaldehyde || 1H Experiment
38 18:15:29 2602051450-0-38-z34413sw 10 PROTON ug2023 + + - + + + + G14-NME2 || 1H Experiment
37 18:06:31 2602051450-0-37-z34413sw 10 PROTON ug2023 + + - + + + + G14-CF3 || 1H Experiment
36 18:00:18 2602051429-0-36-q09060yz 10 PROTON ug2023 + + - + + + + pd(oac)2 yier || 1H Experiment
35 17:54:04 2602051429-0-35-q09060yz 10 PROTON ug2023 + + - + + + + dppf2pdcl2 lydia || 1H Experiment
34 17:50:23 2602051428-0-34-d54865hg 13 C13CPD32 ug2023 - + - - - + + Electrochem -HG || 13C Experiment, 1H decoupled, 32 scans
34 17:48:36 2602051428-0-34-d54865hg 12 P31CPD ug2023 - + - - - + + Electrochem -HG || 31P{1H}, 1H Decoupled, 16 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0; pp: Cannot find any peak for scaling in /mnt/nmrdata/nomad/data/ug2023/nmr/2602051428-0-34-d54865hg/12/pdata/1/peaks
34 17:45:55 2602051428-0-34-d54865hg 11 P31 ug2023 - + - - - + + Electrochem -HG || 31P Experiment, No Decoupling, 32 Scans sref: NUCLEUS '31P' not defined for SOLVENT 'CDCl3' SR is set to 0.0; pp: Cannot find any peak for scaling in /mnt/nmrdata/nomad/data/ug2023/nmr/2602051428-0-34-d54865hg/11/pdata/1/peaks
34 17:37:22 2602051428-0-34-d54865hg 10 PROTON ug2023 + + - + + + + Electrochem -HG || 1H Experiment
33 17:31:10 2602051416-0-33-a98524wr 10 PROTON ug2023 + + - + + + + Jerry Week 1 experiment 1 hexanal || 1H Experiment
32 17:25:06 2602051415-0-32-d98689cd 10 PROTON ug2023 + + - + + + + CD starting material || 1H Experiment
31 17:19:30 2602051351-0-31-s04936gr 10 PROTON ug2023 + + - + + + + flower2 || 1H Experiment
30 17:12:41 2602051349-0-30-z73813ns 10 PROTON ug2023 + + - + + + + Urea D - NS || 1H Experiment
28 17:05:57 2602051345-0-28-s04936gr 10 PROTON ug2023 + + - + + + + flower1 || 1H Experiment
10 16:59:57 2602051345-0-10-s04936gr 10 PROTON ug2023 + + - + + + + manuka3 || 1H Experiment
9 16:53:59 2602051345-0-9-s04936gr 10 PROTON ug2023 + + - + + + + manuka2 || 1H Experiment
7 16:47:36 2602051345-0-7-s04936gr 10 PROTON ug2023 + + - + + + + manuka 1 || 1H Experiment
5 16:41:50 2602051345-0-5-s04936gr 10 PROTON ug2023 + + - + + + + blank || 1H Experiment
4 16:35:11 2602051343-0-4-a98524wr 10 PROTON ug2023 + + - + + + + Joe Week 1 Thursday experiment 1 propanal || 1H Experiment
2 16:27:42 2602051341-0-2-a98524wr 10 PROTON ug2023 + + - + + + + Harry Week 1 Thursday Experiment 1, 4-nitrobenzaldehyde || 1H Experiment
1 16:19:11 2602051337-0-1-a98524wr 10 PROTON ug2023 + + - + + + + Will Week 1 thurs ex 1 benzaldehyde product || 1H Experiment
11 16:12:26 2602051216-0-11-j85765wh 10 PROTON ug2023 + + - + + + + morpholine || 1H Experiment
6 16:04:17 2602051038-0-6-t29189mm 10 PROTON ug2023 + + - + + + + 2bromo2butene || 1H Experiment
3 15:58:21 2602051010-0-3-t69807al 10 PROTON ug2023 + + - + + + + amine B || 1H Experiment
27 15:50:15 2602051332-0-27-e54226ff 10 PROTON ug2023 + + - + + + + 4-methoxyanaline SM || 1H Experiment
26 15:47:19 2602051308-0-26-c68402hw 11 C13CPD32 ug2023 - + - - - + + Urea B Crude ? || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602051308-0-26-c68402hw/11/pdata/1/peaks No peaks found in the specified range.
26 15:41:59 2602051308-0-26-c68402hw 10 PROTON ug2023 + + - + + + + Urea B Crude ? || 1H Experiment
25 15:39:06 2602051306-0-25-b93379br 11 C13CPD32 ug2023 - + - - - + + G12 Reagent Terp || 13C Experiment, 1H decoupled, 32 scans
25 15:32:54 2602051306-0-25-b93379br 10 PROTON ug2023 + + - + + + + G12 Reagent Terp || 1H Experiment
24 15:29:55 2602051306-0-24-b93379br 11 C13CPD32 ug2023 - + - - - + + Group 12 Reagent Limonene || 13C Experiment, 1H decoupled, 32 scans
24 15:22:56 2602051306-0-24-b93379br 10 PROTON ug2023 + + - + + + + Group 12 Reagent Limonene || 1H Experiment
23 15:19:20 2602051254-0-23-z91447bd 11 C13CPD32 ug2023 - + - - - + + Starting mat - Exp 1 - Week 1 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602051254-0-23-z91447bd/11/pdata/1/peaks No peaks found in the specified range.
23 15:13:09 2602051254-0-23-z91447bd 10 PROTON ug2023 + + - + + + + Starting mat - Exp 1 - Week 1 || 1H Experiment
22 15:11:31 2602051236-0-22-d34693sa 12 F19 ug2023 - + - - - + + 4-fluoroaniline || 19F Experiment sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
22 15:08:46 2602051236-0-22-d34693sa 11 PROTON ug2023 - + - - - + + 4-fluoroaniline || 1H Experiment
22 15:02:00 2602051236-0-22-d34693sa 10 C13CPD32 ug2023 + + - + + + + 4-fluoroaniline || 13C Experiment, 1H decoupled, 32 scans
21 14:59:21 2602051236-0-21-d34693sa 11 PROTON ug2023 - + - - - + + aniline || 1H Experiment
21 14:51:02 2602051236-0-21-d34693sa 10 C13CPD32 ug2023 + + - + + + + aniline || 13C Experiment, 1H decoupled, 32 scans
20 14:48:03 2602051234-0-20-d34693sa 11 C13CPD32 ug2023 - + - - - + + 4-methylaniline || 13C Experiment, 1H decoupled, 32 scans
20 14:40:26 2602051234-0-20-d34693sa 10 PROTON ug2023 + + - + + + + 4-methylaniline || 1H Experiment
19 14:37:15 2602051234-0-19-d34693sa 11 C13CPD32 ug2023 - + - - - + + 4-nbutylaniline || 13C Experiment, 1H decoupled, 32 scans
19 14:31:28 2602051234-0-19-d34693sa 10 PROTON ug2023 + + - + + + + 4-nbutylaniline || 1H Experiment
18 14:24:52 2602051220-0-18-k03256gd 10 PROTON ug2023 + + - + + + + Urea C || 1H Experiment
17 14:17:14 2602051220-0-17-t69807al 10 PROTON ug2023 + + - + + + + urea A || 1H Experiment
16 14:08:26 2602051215-0-16-k03256gd 10 PROTON ug2023 + + - + + + + Amine D || 1H Experiment
15 14:02:00 2602051215-0-15-k03256gd 10 PROTON ug2023 + + - + + + + Isocyanide || 1H Experiment
14 13:54:24 2602051216-0-14-j85765wh 10 PROTON ug2023 + + - + + + + 1ethyl || 1H Experiment
13 13:42:13 2602051216-0-13-j85765wh 10 PROTON ug2023 + + - + + + + 4vinylpiridene || 1H Experiment
12 13:34:22 2602051216-0-12-j85765wh 10 PROTON ug2023 + + - + + + + Azaprene || 1H Experiment
12 12:25:04 2602051216-0-12-j85765wh 10 PROTON ug2023 x - - - - - - Azaprene || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
11 12:25:01 2602051216-0-11-j85765wh 10 PROTON ug2023 x - - - - - - morpholine || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
10 12:24:31 2602051216-0-10-j85765wh 10 PROTON ug2023 x - - - - - - piperidene || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Timeout while trying to rotate. Transport FSM is in unexpected state 34: sample is too high for rotation
9 12:17:44 2602051156-0-9-z02649mm 10 PROTON ug2023 + + - + + + + Rotaxane || 1H Experiment
4 12:10:46 2602051011-0-4-t69807al 10 PROTON ug2023 + + - + + + + amine C || 1H Experiment
1 10:48:33 2602051041-0-1-c68402hw 10 PROTON ug2023 x - - - - - - Isocyanate only || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
7 10:48:30 2602051039-0-7-t69807al 10 PROTON ug2023 x - - - - - - amine D || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
6 10:48:15 2602051038-0-6-t29189mm 10 PROTON ug2023 x - - - - - - 2bromo2butene || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Inconsistent Inputs detected by Controller, please check light barriers. SMCB input word: 0x00011B43
5 10:45:24 2602051037-0-5-r99959zh 11 C13CPD32 ug2023 - + - - - + + G3 EE starting material || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602051037-0-5-r99959zh/11/pdata/1/peaks No peaks found in the specified range.
5 10:38:28 2602051037-0-5-r99959zh 10 PROTON ug2023 + + - + + + + G3 EE starting material || 1H Experiment
2 10:28:37 2602051010-0-2-t69807al 10 PROTON ug2023 + + - + + + + amine A || 1H Experiment
13 12:30:21 2602041014-0-13-h93903rc 10 PROTON ug2024 + + - + + + + exp4_RC1 || 1H Experiment
12 12:27:27 2602041014-0-12-y84374bs 11 C13CPD32 ug2024 - + - - - + + BS_exp 4 nmr || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602041014-0-12-y84374bs/11/pdata/1/peaks No peaks found in the specified range.
12 12:18:56 2602041014-0-12-y84374bs 10 PROTON ug2024 + + - + + + + BS_exp 4 nmr || 1H Experiment
11 12:16:04 2602041018-0-11-n84135df 11 C13CPD32 ug2023 - + - - - + + DF_nmr_ex4 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2023/nmr/2602041018-0-11-n84135df/11/pdata/1/peaks No peaks found in the specified range.
11 12:08:56 2602041018-0-11-n84135df 10 PROTON ug2023 + + - + + + + DF_nmr_ex4 || 1H Experiment
10 12:06:05 2602041013-0-10-e34822jd 11 C13CPD32 ug2024 - + - - - + + JD_NMR_Exp4 || 13C Experiment, 1H decoupled, 32 scans
10 11:57:09 2602041013-0-10-e34822jd 10 PROTON ug2024 + + - + + + + JD_NMR_Exp4 || 1H Experiment
9 11:49:36 2602041013-0-9-h93903rc 10 PROTON ug2024 + + - + + + + exp4_RC || 1H Experiment
8 11:42:02 2602041025-0-8-k49220ac 10 PROTON ug2024 + + - + + + + Sadie+Adriana || 1H Experiment
7 11:39:08 2602041012-0-7-w23948mh 11 C13CPD32 ug2024 - + - - - + + MFHEXP4 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602041012-0-7-w23948mh/11/pdata/1/peaks No peaks found in the specified range.
7 11:32:26 2602041012-0-7-w23948mh 10 PROTON ug2024 + + - + + + + MFHEXP4 || 1H Experiment
6 11:26:19 2602041059-0-6-y15874hk 11 COSYGPSW ug2024 - + - - - + + Hibi Exp14 || COSY
6 11:20:10 2602041059-0-6-y15874hk 10 PROTON ug2024 + + - + + + + Hibi Exp14 || 1H Experiment
5 11:17:15 2602041010-0-5-z58535ek 11 C13CPD32 ug2024 - + - - - + + EKCexp4 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602041010-0-5-z58535ek/11/pdata/1/peaks No peaks found in the specified range.
5 11:09:48 2602041010-0-5-z58535ek 10 PROTON ug2024 + + - + + + + EKCexp4 || 1H Experiment
4 11:03:40 2602041048-0-4-p15738ht 11 COSYGPSW ug2024 - + - - - + + HarveyTiteEx14Sample || COSY
4 10:57:05 2602041048-0-4-p15738ht 10 PROTON ug2024 + + - + + + + HarveyTiteEx14Sample || COSY
3 10:44:58 2602041040-0-3-r20601bc 10 PROTON ug2024 + + - + + + + EXP14 sample BC || 1H Experiment
2 10:41:41 2602041028-0-2-g51418ja 11 C13CPD32 ug2024 - + - - - + + Lily Anderton X4 || 13C Experiment, 1H decoupled, 32 scans pp: Unable to assign a peak for scaling of /mnt/nmrdata/nomad/data/ug2024/nmr/2602041028-0-2-g51418ja/11/pdata/1/peaks No peaks found in the specified range.
2 10:34:14 2602041028-0-2-g51418ja 10 PROTON ug2024 + + - + + + + Lily Anderton X4 || 1H Experiment
7 10:32:42 2602041012-0-7-w23948mh 10 PROTON ug2024 x - - - - - - MFHEXP4 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
5 10:32:39 2602041010-0-5-z58535ek 10 PROTON ug2024 x - - - - - - EKCexp4 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
2 10:32:34 2602041028-0-2-g51418ja 10 PROTON ug2024 x - - - - - - Lily Anderton X4 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
7 10:31:29 2602041012-0-7-w23948mh 10 PROTON ug2024 x - - - - - - MFHEXP4 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
5 10:31:26 2602041010-0-5-z58535ek 10 PROTON ug2024 x - - - - - - EKCexp4 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: System is not ready to accept new command
2 10:30:47 2602041028-0-2-g51418ja 10 PROTON ug2024 x - - - - - - Lily Anderton X4 || 1H Experiment SampleChanger Error: 1000 STOP_CHANGER SampleTransporter: Timeout while trying to rotate. Transport FSM is in unexpected state 34: sample is too high for rotation
1 10:21:17 2602041009-0-1-j00738ta 10 PROTON ug2024 + + - + + + + TA SM || 1H Experiment
09:08:39 Start-Up - - - - - - - Automation was stopped by user