IconNMR Automation Run Status: | |
Day Experiments: | 00:00 |
Busy Until: | Wed 14:03 |
Night Experiments: | 00:00 |
Holder | Status | Name | ExpNo | Experiment | User | Time | Title |
60 | Error | 20230427_B300-2.044_-60 | 10 | N PROTON 1H exp. 16 scans | nmrsu | 00:01:55 |
Holder | Time | Name | ExpNo | Experiment | User | Load | Atma | Spin | Lock | Shim | Acq | Proc | Title | Remarks |
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
60 | 13:53:10 | 20230427_B300-2.044_-60 | 10 | PROTON | nmrsu | + | - | + | x | - | - | - | Lock failed after multiple attempts, flock: Results: Solvent: CDCl3 Inconsistent number of peaks !! Number of solvent peaks found: 78 Using largest peak at ppm: 11.00 Chemical Shift of defined solvent: 7.24 Current lock field: 3616 New lockfield: 3420, flock autolock timeout after 30 seconds., Results: Solvent: CDCl3 Inconsistent number of peaks !! Number of solvent peaks found: 37 Using largest peak at ppm: 10.39 Chemical Shift of defined solvent: 7.24 Current lock field: 3616 New lockfield: 3452, flock autolock timeout after 30 seconds., Automation was stopped |